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(1 - 19 of 19)
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Tirumalasetty, G.K. (author), Van Huis, M.A. (author), Kwakernaak, C. (author), Sietsma, J. (author), Sloof, W.G. (author), Zandbergen, H.W. (author)
A combination of Electron Back-Scattered Diffraction (EBSD) and high-sensitivity Electron Probe Micro-Analysis (EPMA) was used to correlate the changes in microstructural features upon deformation with local chemical composition in Transformation-Induced Plasticity steels. A novel cleaning procedure was developed that allows complete monitoring...
journal article 2013
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Tirumalasetty, G.K. (author), Fang, C.M. (author), Xu, Q. (author), Jansen, J. (author), Sietsma, J. (author), Van Huis, M.A. (author), Zandbergen, H.W. (author)
A transmission electron microscopy study was conducted on nanoprecipitates formed in Ti microalloyed transformation-inducedplasticity-assisted steels, revealing the presence of Ti(N), Ti2CS and a novel type of ultra-fine Fe(C) precipitate. The matrix/precipitate orientation relationships, sizes and shapes were investigated in detail. The...
journal article 2012
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Tirumalasetty, G.K. (author), Van Huis, M.A. (author), Kwakernaak, C. (author), Sietsma, J. (author), Sloof, W.G. (author), Zandbergen, H.W. (author)
Uniaxial straining experiments were performed on a rolled and annealed Si-alloyed TRIP (transformation-induced plasticity) steel sheet in order to assess the role of its microstructure on the mechanical stability of austenite grains with respect to martensitic transformation. The transformation behavior of individual metastable austenite grains...
journal article 2012
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Tirumalasetty, G.K. (author), Van Huis, M.A. (author), Fang, C.M. (author), Xu, Q. (author), Tichelaar, F.D. (author), Hanlon, D.N. (author), Sietsma, J. (author), Zandbergen, H.W. (author)
Multiphase steels utilising composite strengthening may be further strengthened via grain refinement or precipitation by the addition of microalloying elements. In this study a Nb microalloyed steel comprising martensite, bainite and retained austenite has been studied. By means of transmission electron microscopy (TEM), we have investigated the...
journal article 2011
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Giang, N. (author), Xu, Q. (author), Hor, Y.S. (author), Williams, A.J. (author), Dutton, S.E. (author), Zandbergen, H.W. (author), Cava, R.J. (author)
The structural misfit compound (PbSe)1.16(TiSe2)2 is reported. It is a superconductor with a Tc of 2.3 K. (PbSe)1.16(TiSe2)2 derives from a parent compound, TiSe2, which shows a charge-density wave transition and no superconductivity. The crystal structure, characterized by high-resolution electron microscopy and powder x-ray diffraction,...
journal article 2010
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Hor, Y.S. (author), Williams, A.J. (author), Checkelsky, J.G. (author), Roushan, P. (author), Seo, J. (author), Xu, Q. (author), Zandbergen, H.W. (author), Yazdani, A. (author), Ong, N.P. (author), Cava, R.J. (author)
Bi2Se3 is one of a handful of known topological insulators. Here we show that copper intercalation in the van der Waals gaps between the Bi2Se3 layers, yielding an electron concentration of ?2×1020??cm-3, results in superconductivity at 3.8 K in CuxBi2Se3 for 0.12?x?0.15. This demonstrates that Cooper pairing is possible in Bi2Se3 at accessible...
journal article 2010
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Fang, C.M. (author), Van Huis, M.A. (author), Zandbergen, H.W. (author)
The iron carbide Fe7C3 exhibits two types of basic crystal structures, an orthorhombic (o-) form and a hexagonal (h-) one. First-principles calculations have been performed for the basic Fe7C3 forms and for the related ?-Fe3C cementite phase. Accurate total-energy calculations show that the stability of Fe7C3 is comparable to that of ?-Fe3C. The...
journal article 2009
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Holman, K.L. (author), McQueen, T.M. (author), Williams, A.J. (author), Klimczuk, T. (author), Stephens, P.W. (author), Zandbergen, H.W. (author), Xu, Q. (author), Ronning, F. (author), Cava, R.J. (author)
Although many materials display the transition from insulating to metallic behavior on doping, only a few, such as VO2, have the right combination of crystal structure and physical properties to serve as model systems. Here we report the electronic and structural characteristics of the insulator to metal transition in V1?xMoxO2, which we have...
journal article 2009
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McQueen, T.M. (author), Huang, Q. (author), Ksenofontov, V. (author), Felser, C. (author), Xu, Q. (author), Zandbergen, H. (author), Hor, Y.S. (author), Allred, J. (author), Williams, A.J. (author), Qu, D. (author), Checkelsky, J. (author), Ong, N.P. (author), Cava, R.J. (author)
The recently discovered iron arsenide superconductors appear to display a universal set of characteristic features, including proximity to a magnetically ordered state and robustness of the superconductivity in the presence of disorder. Here we show that superconductivity in Fe1+?Se, which can be considered the parent compound of the...
journal article 2009
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Wagner, K.E. (author), Morosan, E. (author), Hor, Y.S. (author), Tao, J. (author), Zhu, Y. (author), Sanders, T. (author), McQueen, T.M. (author), Zandbergen, H.W. (author), Williams, A.J. (author), West, D.V. (author), Cava, R.J. (author)
We report the characterization of layered 2H-type CuxTaS2 for 0?x?0.12. The charge density wave (CDW), at 70 K for TaS2, is destabilized with Cu doping. The sub-1 K superconducting transition in undoped 2H-TaS2 jumps quickly to 2.5 K at low x, increases to 4.5 K at the optimal composition Cu0.04TaS2, and then decreases at higher x. The...
journal article 2008
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Heersche, H.B. (author), Lientschnig, G. (author), O'Neill, K. (author), Van der Zant, H.S.J. (author), Zandbergen, H.W. (author)
The authors imaged electromigration-induced nanogap formation in situ by transmission electron microscopy. Real-time video recordings show that edge voids form near the cathode side. The polycrystalline gold wires narrow down until a single-grain boundary intersects the constriction along which the breaking continues. During the last 50?ms of...
journal article 2007
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Klimczuk, T. (author), Xu, Q. (author), Morosan, E. (author), Thompson, J.D. (author), Zandbergen, H.W. (author), Cava, R.J. (author)
Mg10Ir19B16, a previously unreported compound in the Mg-Ir-B chemical system, is found to be superconducting at temperatures near 5 K. The fact that the compound exhibits a range of superconducting temperatures between 4 and 5 K suggests that a range of stoichiometries is allowed, though no structural evidence for this is observed. The compound...
journal article 2006
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Bos, J.W.G. (author), Lee, M. (author), Morosan, E. (author), Zandbergen, H.W. (author), Lee, W.L. (author), Ong, N.P. (author), Cava, R.J. (author)
Ferromagnetism is observed below 10 K in [Bi0.75Te0.125Mn0.125]Te. This material has the BiTe structure, which is made from the stacking of two Te-Bi-Te-Bi-Te blocks and one Bi-Bi block per unit cell. Crystal structure analysis shows that Mn is localized in the Bi2 blocks, and is accompanied by an equal amount of TeBi antisite occupancy in the...
journal article 2006
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Balicas, L. (author), Analytis, J.G. (author), Jo, Y.J. (author), Storr, K. (author), Zandbergen, H. (author), Xin, Y. (author), Hussey, N.E. (author), Chou, F.C. (author), Lee, P.A. (author)
Shubnikov–de Haas oscillations for two well-defined frequencies, corresponding, respectively, to areas of 0.8 and 1.36% of the first Brillouin zone, were observed in single crystals of Na0.3CoO2. The existence of Na superstructures in Na0.3CoO2, coupled with this observation, suggests the possibility that the periods are due to the...
journal article 2006
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Yang, Z.Q. (author), Zhang, Y.Q. (author), Aarts, J. (author), Wu, M.Y. (author), Zandbergen, H.W. (author)
We report the effects of biaxial strain on the charge ordering temperature Tco of the mixed-valent manganite perovskite oxide Pr0.5Ca0.5MnO3. Thin films were grown on SrTiO3, which has a 1.3% larger in-plane lattice parameter. Other substrates were used for comparison. Transport measurements combined with data from electron microscopy show that...
journal article 2006
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Wu, M.Y. (author), Krapf, D. (author), Zandbergen, M. (author), Zandbergen, H. (author), Batson, P.E. (author)
An electron beam can drill nanopores in SiO2 or silicon nitride membranes and shrink a pore to a smaller diameter. Such nanopores are promising for single molecule detection. The pore formation in a 40?nm thick silicon nitride?SiO2 bilayer using an electron beam with a diameter of 8?nm (full width of half height) was investigated by electron...
journal article 2005
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Storm, A.J. (author), Chen, J.H. (author), Ling, X.S. (author), Zandbergen, H.W. (author), Dekker, C. (author)
The imaging beam of a transmission electron microscope can be used to fine tune critical dimensions in silicon oxide nanostructures. This technique is particularly useful for the fabrication of nanopores with single-nanometer precision, down to 2 nm. We report a detailed study on the effect of electron-beam irradiation on apertures with various...
journal article 2005
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Lazar, S. (author), Weyher, J.L. (author), Macht, L. (author), Tichelaar, F.D. (author), Zandbergen, H.W. (author)
Photochemical (PEC) etching and transmission electron microscopy (TEM) have been used to study the defects in hetero-epitaxial GaN layers. TEM proved that PEC etching reveals not only dislocations but also nanopipes in the form of protruding, whisker-like etch features. It is shown by diffraction contrast techniques that the nanopipes are screw...
journal article 2004
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Pedarnig, J.D. (author), Rössler, R. (author), Delamare, M.P. (author), Lang, W. (author), Bäuerle, D. (author), Köhler, A. (author), Zandbergen, H.W. (author)
Vicinal YBa2Cu3O7?? (YBCO) thin films of thickness h = 20–480?nm are grown by pulsed-laser deposition on 10° miscut (001) SrTiO3 substrates. The anisotropic resistivities, c-axis texture, and critical temperature drastically depend on the thickness of vicinal films. High-resolution electron microscopy reveals a defect microstructure with strong...
journal article 2002
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