Microalloyed steels strengthened by precipitates nucleated during the austenite (γ) to ferrite (α) phase transformation can provide steel producers with a new type of High Strength Low Alloy (HSLA) steel suitable for increasing demands for their properties. To better understand the conditions at the migrating α/γ interface, which can lead to said precipitation, the kinetics of the phase transformations are investigated.
Three different microalloyed steels with the same amount of manganese and varying amounts of carbon and vanadium are analysed on four different annealing temperatures. Experimental data on the phase transformation kinetics is obtained through dilatometry. A quantitative solute drag model is developed and tested on the quaternary alloys to obtain data on energy dissipation due to segregation of the substitutional elements. A theory is postulated to relate the experimental data and related obtained interface velocities to the modelling results.
Experimental results vary greatly, but at medium (650°C) to high (750°C) annealing temperatures an increase of vanadium and carbon content leads to a slower transformation compared to the alloy with lower concentrations of said elements.
Modelling results indicate that energy dissipation due to vanadium is minimal, especially relative to that of manganese. This means that observed changes in transformation dynamics for the alloys with changing vanadium and carbon content have to be understood in terms of vanadium-carbide precipitation behaviour and related elemental consumption, and not in energy dissipation due to vanadium segregation.

The present study investigates the microstructural evolution of Sn-Ag-Cu (SAC) solder joints subjected to thermal cycling, with emphasis on recrystallization and grain orientation. Thermal cycling is the main failure source in reliability tests of electronic devices, yet its microstructural effects remain insufficiently understood. Although numerous studies have examined solder joint fatigue using numerical modeling, the early microstructural changes are often overlooked. To address this gap, the present work characterizes experimentally stages of thermal-cycling-induced microstructural evolution.
The evolution of SAC solder joints was characterized using Electron Backscatter Diffraction (EBSD) on two sets of samples. (i) joints thermally cycled for an increasing number of cycles and subsequently cross sectioned, and (ii) pre-cross-sectioned joints analyzed after consecutive rounds of cycling. Two distinct recrystallization mechanisms, namely primary and continuous dynamic, were identified, stabilizing after three thermal cycling stages. Grain rotation toward the [001]Sn-substrate angle and activation of slip systems 4, 6, and 10 suggest a strong link to the initial reflow texture. Moreover, IMC coarsening which facilitates grain boundary unpinning and promotes crack initiation, was also observed. Recrystallized grains exhibited a decrease in Young's Modulus, likely associated with orientation effects.
Calculation of Geometrically Necessary Dislocation (GND) density and Stored Energy Density (SED), with the aim to link EBSD and numerical modeling, while adequate for a first estimation, showcases the need for improved integration methods. Finally, the use of pre-cross-sectioned samples for in situ study of microstructural evolution is not recommended due to stress relaxation effects.