Microstructural Study of Ultra-High Temperature Ceramic Matrix Composites Synthesized Via Reactive Melt Infiltration

Master Thesis (2025)
Author(s)

A.R. Kode (TU Delft - Aerospace Engineering)

Contributor(s)

Y. Tang – Mentor (TU Delft - Group Tang)

Y. van Haaren – Mentor (Arceon)

Baris Kumru – Graduation committee member (TU Delft - Group Kumru)

J.A. Pascoe – Graduation committee member (TU Delft - Group Pascoe)

Faculty
Aerospace Engineering
More Info
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Publication Year
2025
Language
English
Graduation Date
09-07-2025
Awarding Institution
Delft University of Technology
Programme
['Aerospace Engineering']
Sponsors
Arceon
Faculty
Aerospace Engineering
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Abstract

This research investigates the influence of Ultra-High Temperature Ceramic (UHTC) additives on the microstructure and oxidation behavior of Ceramic Matrix Composites (CMCs) synthesized via Reactive Melt Infiltration (RMI). The study focuses on three key parameters of the UHTC additives: particle size, additive volume, and chemical composition. Comprehensive material characterization was conducted throughout the RMI process to study the relationships between these parameters and the resulting microstructural quality. The synthesized samples were subjected to furnace oxidation tests at 1000°C and 1200°C over varying exposure durations. The experimental results demonstrated the oxidation response of ZrB2- and ZrC-based UHTCMC materials produced by RMI, providing insights into optimizing additive selection and processing conditions for improved (ultra)-high temperature application.

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File under embargo until 09-07-2027