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van Heijst, S.E. (author)Two-dimensional (2D) layered materials have attracted the interest of the scientific community following the discovery of graphene and its extraordinary properties. Of particular interest is a class of materials called transition metal dichalcogenides (TMDs). The materials within this class were discovered to show similarly...doctoral thesis 2024
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Schneider, Mike (author), Couzinié, Jean Philippe (author), Shalabi, Amin (author), Ibrahimkhel, Farhad (author), Ferrari, A. (author), Körmann, F.H.W. (author), Laplanche, Guillaume (author)This work aims to predict the microstructure of recrystallized medium and high-entropy alloys (MEAs and HEAs) with a face-centered cubic structure, in particular the density of annealing twins and their thickness. Eight MEAs and five HEAs from the Cr-Mn-Fe-Co-Ni system are considered, which have been cast, homogenized, cold-worked and...journal article 2024
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Oñoro, M. (author), de Castro, V. (author), Leguey, T. (author), Pöpperlová, J. (author), Huizenga, R.M. (author), Auger, M. A. (author)An oxide dispersion strengthened (ODS) steel with nominal composition Fe–14Cr–2W–0.4Ti–0.3Y<sub>2</sub>O<sub>3</sub> (wt%) has been manufactured by mechanical alloying of pre-alloyed powders with nanosized Y<sub>2</sub>O<sub>3</sub>, compacted by hot isostatic pressing and hot cross rolled. In order to evaluate the long-term thermal...journal article 2024
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Nikolic, Ksenija (author), Mattos Ferreira, V. (author), Malet, Loïc (author), Depover, Tom (author), Verbeken, Kim (author), Petrov, R.H. (author)The microstructure of a damaged bearing from the field was characterized in this work with the intention to better understand microstructural features behind formation of White Etching Cracks (WEC) in bearings. Microstructural characterization of the altered white etching area (WEA) involved conventional electron backscattered diffraction ...journal article 2023
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Nutter, John (author), Qi, Jiahui (author), Farahani, H. (author), Rainforth, W. Mark (author), van der Zwaag, S. (author)The current study reports in situ TEM observations of the growth of bainitic ferrite in an Fe-0.3C-3Mn-1.5Si-0.15Mo steel held isothermally at 300 °C with a higher spatio-temporal resolution than in previous studies. Significant variations were found in the lengthening rate, with the highest being in excess of 30,000 nm.s<sup>−1</sup> while...journal article 2023
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Zhang, Y. (author), Copuroglu, Oguzhan (author)Through the integration of SEM-BSE and TEM, we gained a comprehensive 3-dimensional understanding of different distribution patterns of inner hydration products of slag. For fully hydrated small slag grains, two distinct sub-zones were formed in the rims. Lath-like, well-crystalline hydrotalcite-like crystals were found to precipitate, grow,...journal article 2023
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Zhang, Y. (author), Zhang, Shizhe (author), Liu, C. (author), Copuroglu, Oguzhan (author)In this paper, the authors characterized two types of zonation within slag rims in aged alkali-activated slag (AAS) systems through SEM and TEM technology. These two elemental zonation were closely related to the pore structure of AAS pastes, thus providing strong implication for the transport- and durability-related performance of AAS...journal article 2023
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Skoupý, R. (author), Boltje, D.B. (author), Slouf, Miroslav (author), Mrázová, Kateřina (author), Láznička, Tomáš (author), Taisne, C.M. (author), Krzyžánek, Vladislav (author), Hoogenboom, J.P. (author), Jakobi, A. (author)A quantitative four-dimensional scanning transmission electron microscopy (4D-STEM) imaging technique (q4STEM) for local thickness estimation across amorphous specimen such as obtained by focused ion beam (FIB)-milling of lamellae for (cryo-)TEM analysis is presented. This study is based on measuring spatially resolved diffraction patterns to...journal article 2023
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Ferrero, Riccardo (author), Androulakis, Ioannis (author), Martino, Luca (author), Nadar, R.A. (author), van Rhoon, G.C. (author), Manzin, Alessandra (author)The evaluation of the biological effects of therapeutic hyperthermia in oncology and the precise quantification of thermal dose, when heating is coupled with radiotherapy or chemotherapy, are active fields of research. The reliable measurement of hyperthermia effects on cells and tissues requires a strong control of the delivered power and of...journal article 2022
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Kosari, A. (author)For many decades, corrosion and corrosion inhibition of high-strength aluminium alloys have been studied indirectly and through traditional and separately performed electrochemical, spectroscopic and microscopic techniques. These approaches employed to date commonly lack sufficient lateral and time resolution to unravel early-stage events which...doctoral thesis 2021
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Kosari, A. (author), Tichelaar, F.D. (author), Visser, P. (author), Zandbergen, H.W. (author), Terryn, H.A. (author), Mol, J.M.C. (author)Lithium leaching coatings have recently been developed as eco-friendly active corrosion protection technology for aerospace aluminium alloys (AAs) by the formation of a conversion layer at coating defects. While general conversion layer formation characteristics were studied and reported before, here we study the local layer formation process...journal article 2021
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Kosari, A. (author), Zandbergen, H.W. (author), Tichelaar, F.D. (author), Visser, P. (author), Terryn, H.A. (author), Mol, J.M.C. (author)Liquid-phase transmission electron microscopy (LP-TEM) has provided corrosion scientists with a unique opportunity to directly correlate nanoscopic morphological and compositional evolutions to the corresponding electrochemical response of corroding thin TEM specimens. Electrochemical liquid cell designs are key components of a LP-TEM study...journal article 2021
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Rogal, Lukasz (author), Ikeda, Yuji (author), Lai, Minjie (author), Körmann, F.H.W. (author), Kalinowska, Alicja (author), Grabowski, Blazej (author)High entropy alloys (HEAs) in the hexagonal close-packed (hcp) phase usually show poor mechanical properties. We demonstrate here, by use of ab initio simulations and detailed experimental investigations, that the mechanical properties can be improved by optimizing the microstructure. In particular we design a dual-phase HEA consisting of a...journal article 2020
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Kosari, A. (author), Visser, P. (author), Tichelaar, F.D. (author), Eswara, S. (author), Audinot, J. N. (author), Wirtz, T. (author), Zandbergen, H.W. (author), Terryn, H.A. (author), Mol, J.M.C. (author)This work focuses on the cross-sectional characterization of the protective conversion layer formed on AA2024-T3 by lithium-leaching from a polyurethane coating in a corrosive environment. The layer shows a multi-layered arrangement comprising nanoscopic local phases. Transmission electron microscopy (TEM) and complementary high-resolution...journal article 2020
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Kosari, A. (author), Zandbergen, H.W. (author), Tichelaar, F.D. (author), Visser, P. (author), Terryn, H.A. (author), Mol, J.M.C. (author)Identifying corrosion initiation events in metals and alloys demands techniques that can provide temporal and spatial resolution simultaneously. Transmission electron microscopy (TEM) enables one to obtain microstructural and chemical descriptors of materials at atomic/nanoscopic level and has been used in corrosion studies of many metal...review 2020
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Basak, S. (author), Migunov, Vadim (author), Lee, Q. (author), Ganapathy, S. (author), Vijay, Ashwin (author), Ooms, F.G.B. (author), Wagemaker, M. (author), Kelder, E.M. (author), Arszelewska, Violetta (author)With operando transmission electron microscopy visualizing the solid-solid electrode-electrolyte interface of silicon active particles and lithium oxide solid electrolyte as a model system, we show that (de)lithiation (battery cycling) does not require all particles to be in direct contact with electrolytes across length scales of a few...journal article 2020
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Kosari, A. (author), Zandbergen, H.W. (author), Tichelaar, F.D. (author), Visser, P. (author), Taheri, P. (author), Terryn, H.A. (author), Mol, J.M.C. (author)Dealloying is involved in materials science responsible for fabrication of nanoscale structures beneficially but for corrosion degradations detrimentally. Detailed understanding related to the latter is critical for designing corrosion-resistance alloys and dedicated inhibition systems. Thus, direct nanoscopic observations of nano-structural...journal article 2020
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Kosari, A. (author), Tichelaar, F.D. (author), Visser, P. (author), Zandbergen, H.W. (author), Terryn, H.A. (author), Mol, J.M.C. (author)Nanoscopic characterization of heterogeneous intermetallic particles (IMPs) which microstructurally and compositionally evolve during local corrosion is crucial in unravelling the mechanisms and sequence of initial and local corrosion events. Herein, we study site-specific initiation events focused on microscopic constituent intermetallic...journal article 2020
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Eftekharimilani, P. (author)The potential for weight reduction, ease of manufacturing and improved crashworthiness makes advanced and ultra high strength steels attractive for automotive applications. Resistance spot welding is by far the most widely used joining method in the automotive industry due to the high operating speeds, the reliability of the process and the...doctoral thesis 2019
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He, Xuanmin (author)The Nobel Prize in Chemistry in 2017 went to the development of cryo-electron microscopy, which contributed to the discovery of new cells and viruses, the diagnosis of unknown diseases, the mapping of human genomes and the manufacturing of semiconductors. Cryo Correlative light and electron microscopy (Cryo-CLEM), is the combination of using...master thesis 2019
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