Development of a new generation of quench and partitioning steels
Influence of processing parameters on texture, nanoindentation, and mechanical properties
E. A. Ariza-Echeverri (Universidade de São Paulo)
M. Masoumi (Center of Engineering, Modelling and Applied Social Sciences)
A. S. Nishikawa (Universidade de São Paulo, TU Delft - (OLD) MSE-3)
D. H. Mesa (Universidad Tecnológica de Pereira)
A. E. Marquez-Rossy (Oak Ridge National Laboratory)
André Paulo Tschiptschin (Universidade de São Paulo)
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Abstract
A novel quenching and partitioning process (Q&P) including the hot stamping (HS) process was studied, using two stamping temperatures (750 °C and 800 °C) and two quenching temperatures (318 °C and 328 °C). This combination is here called Hot Stamping and Quenching and Partitioning process (HSQ&P). The partitioning step was performed at 400 °C for 100 s in all cycles. Microstructural features were comprehensively studied using electron backscattered diffraction and nanoindentation techniques. HSQ&P samples showed a good combination of ductility and high-strength due to the presence of: retained austenite, inter-critical ferrite with low stored internal strain energy, grain refinement via DIFT-effect (deformation induced ferrite transformation), martensite, and bainite. Significant internal stress relief was caused by carbon partitioning, which was induced by the DIFT-effect and the partitioning stage. This also led to a considerable stored energy, which was characterized by the Kernel average dislocation and geometrically necessary dislocation analysis. In addition, predominant {110}//strain direction crystallographic texture was identified, which promotes slip deformation and enhances the mechanical properties. Moreover, remarkable amounts of fine film-like retained austenite oriented along compact crystallographic directions (i.e., 〈111〉 and 〈112〉) were observed. Finally, subsize tensile test verified the optimum mechanical behavior of HSQ&P specimens.
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