Cost-effective and efficient preparation of FePO4 electrodes from spent LiFePO4 batteries for enhanced lithium extraction from salt lakes

Journal Article (2025)
Author(s)

Yawen Gao (Cheng Du University of Technology)

Luxiang Ma (Cheng Du University of Technology)

Shuaifei Zhao (Deakin University)

Chunxi Hai (Cheng Du University of Technology)

Tiandong Chen (Cheng Du University of Technology)

Junyi Zhang (Cheng Du University of Technology)

Yan Zhao (Cheng Du University of Technology)

Yanxia Sun (Cheng Du University of Technology)

Shengde Dong (Cheng Du University of Technology)

Xin He (Cheng Du University of Technology)

Qi Xu (Cheng Du University of Technology)

Xiaowang Wu (Qinghai Zhongxin Guoan Lithium Development Co., Ltd.)

Caixiong Quan (Qinghai Zhongxin Guoan Lithium Development Co., Ltd.)

Hongli Su (TU Delft - Civil Engineering & Geosciences)

Yuan Zhou (Cheng Du University of Technology)

Research Group
Resources & Recycling
DOI related publication
https://doi.org/10.1016/j.mtener.2025.101848 Final published version
More Info
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Publication Year
2025
Language
English
Research Group
Resources & Recycling
Bibliographical Note
Green Open Access added to TU Delft Institutional Repository ‘You share, we take care!’ – Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public.
Journal title
Materials Today Energy
Volume number
50
Article number
101848
Downloads counter
234
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Abstract

Cost-effective and efficient lithium extraction technology is vital to foster the growth of lithium industry. This paper proposed a novel approach for the high value utilization of spent LiFePO4 (S-LiFePO4) in the field of lithium extraction from salt lakes was proposed using spent LiFePO4 (S-LiFePO4) as raw material. The anode, made from spent LiFePO4, is prepared via a sintering process, while FePO4, obtained through chemical oxidation, is used as the cathode. Compared with commercial LiFePO4, this system not only reduces the cost but also greatly shortens the preparation time of FePO4 (only about 10min is required). And the electrochemical extraction system had a favorable lithium extraction capacity (29.25 mg/g) from actual brine, reducing the Mg/Li ratio from 61.4 to 0.8. This study not only achieved the low-cost preparation of electrode materials and facilitated the large-scale implementation of this process, but also proposed a high-value comprehensive utilization strategy for lithium-ion batteries recycling.

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