Analysis of differential scanning calorimetry (DSC): determining the transition temperatures, and enthalpy and heat capacity changes in multicomponent systems by analytical model fitting

We have developed an analytical method to quantitatively analyze differential scanning calorimetry (DSC) experimental data. This method provides accurate determination of thermal properties such as equilibrium melting temperature, latent heat, change of heat capacity which can be performed automatically without intervention of a DSC operator....

Rheological and Microstructural Assessment of Complex Bituminous Binders [PPT]

In the past years, the use of liquid additives as bitumen modifiers has increased to enhance or adjust the properties of bitumen for wide range of applications. Their molecular composition and mutual interaction result in a specific phase morphology in the binders. Hence, there is a need to evaluate the phase and interphase framework and...

The creep performance of bio-based and synthetic lining adhesives at different environmental conditions

Canvas paintings are prone to environmental ageing. Hence, the structural conservation of canvas paintings may require lining, a process in which a secondary canvas is adhered to the reverse of the damaged original canvas to provide additional support. Choosing the optimum adhesive in combination with a lining method is crucial and yet...

Molten Salt Reactor Chemistry: Structure and Equilibria

Molten salts are a class of ionic liquids which have in recent years been the focus of extensive fundamental research given that they are a versatile class of reaction media with a variety of appealing thermophysical and thermochemical properties (e.g. melting points, heat capacities, vapor pressures, densities, thermal conductivities, etc..)...

Mechanical Behaviour of PA2241FR used in Selective Laser Sintering

This research focuses on the possible causes of variation in the tensile strength and stiffness of witness specimens that are used in the manufacturing of aerospace grade selective laser sintered parts. Using specimens and data obtained from Materialise of the PA2241FR samples, the crystallinity and porosity of the samples was determined. The...

The Set-Invariance Paradigm in Fuzzy Adaptive DSC Design of Large-Scale Nonlinear Input-Constrained Systems

This paper proposes a novel set-invariance adaptive dynamic surface control (DSC) design for a larger class of uncertain large-scale nonlinear input-saturated systems. The peculiarity of this class is that no a priori bound on the continuous control gain functions is assumed (i.e., their boundedness cannot be assumed before obtaining system...

Mechanical and physical characterization of natural and synthetic consolidants

The mechanical behavior of adhesives is strongly influenced by a large number of variables, relating to a complex interaction of mechanical-physical-chemical factors, such as its loading direction (shear, peel), the temperature and the environmental relative humidity (RH). These variables can have a large influence on the durability of...

Nonlinear Systems with Uncertain Periodically Disturbed Control Gain Functions: Adaptive Fuzzy Control with Invariance Properties

This paper proposes a novel adaptive fuzzy dynamic surface control (DSC) method for an extended class of periodically disturbed strict-feedback nonlinear systems. The peculiarity of this extended class is that the control gain functions are not bounded a priori but simply taken to be continuous and with a known sign. In contrast with existing...

Effect of ultrasonic welding process on the crystallinity at the welding interface of CF/PPS joints

The influence of the ultrasonic welding process parameters, namely the force and the vibration amplitude, on the crystallinity degree at the welding interface of CF/PPS (carbon fibre reinforced poly(phenylene) sulphide) joints is investigated. Two different sets of parameters, one representing high force and high vibration amplitude (1000 N,...

On the use of Laser Speckle Imaging to study local polymer dynamics

Effects of Thermal Degradation on Carbon Reinforced PEEK Composites

The application of fibre reinforced thermoplastic composites in aerospace industry has increased drastically in the last decade. Carbon fibre/Polyether-ether-ketone (C/PEEK) is one of the high-performance thermoplastic composites and is replacing metallic and thermosetting counterparts in various aircrafts components. Parts made from such...

Predicting the Mechanical Properties of Animal Glue Thin Films

This report shows that animal glue from porcine skins can be used to make thin films with reproducible properties. It shows that the tensile strength of the film relates linearly to the bloom strength, while the stiffness remains constant for temperatures lower than the glass transition temperature. The report continues to show how Differential...

Analyzing Protein Denaturation using Fast Differential Scanning Calorimetry

This paper investigates the possibility to measure protein denaturation with Fast Differential Scanning Calorimetry (FDSC). Cancer can be diagnosed by measuring protein denaturation in blood plasma using Differential Scanning Calorimetry (DSC). FDSC can reduce diagnosis time from hours to minutes, requiring significantly smaller sample...

Electrical and interfacial properties of a Li3Fe2(PO4)3 single crystal with silver electrodes