The current study reports in situ TEM observations of the growth of bainitic ferrite in an Fe-0.3C-3Mn-1.5Si-0.15Mo steel held isothermally at 300 °C with a higher spatio-temporal resolution than in previous studies. Significant variations were found in the lengthening rate, with the highest being in excess of 30,000 nm.s−1 while more common lengthening rates of 10–1000 nm.s−1 provided the highest quality observations. Both sheaves with visible sub units and individual laths were observed during growth with the lengthening behaviour of sheaves found to be discontinuous - in the most favourably oriented sheave this could be linked to sub unit behaviour. The transformation behaviour was comparable to that of HT-LSCM observations of bainitic ferrite growth for the most comparable steel compositions and to ‘textbook’ descriptions of the formation of bainite sheaves. In addition, other relevant phenomena were recorded, including the generation and movement of dislocations in the austenite during transformation, the interaction of laths with twin boundaries and the initially slow growth of bainitic ferrite laths.@en

The kinetic behaviour of austenite/ferrite interfaces in a low carbon – 0.5 mass% Mn containing steel during Cyclic Partial Phase Transformation (CPPT) experiments has been investigated using hot stage Transmission Electron Microscopy (TEM). Individual interfaces were observed to display behaviour typical of CPPT experiments as recorded in macroscopic dilatometry experiments and demonstrated i) the “normal”, ii) inverse transformations and iii) a stagnant stage in which the interface migrates at a very low velocity as a result of the interface passing through a Mn enriched zone due to the preceding transformation. The length of the stagnant stage determined from the TEM observations shows excellent agreement with that measured from dilatometry and kinetic modelling, whilst the distance migrated from the interface shows some disparities which are primarily attributed to differences in assumptions about grain geometry and nucleation. No special interface features were observed when the interface changed direction and passed through the previously Mn-enriched zones. General observations on the interaction of the transformation interface with microstructural features are also reported.@en

The current study reports the detailed analysis of an observation of the local pinning of a slowly moving austenite-ferrite interface by a single nanosized oxidic particle. The observations were made during an in situ cyclic partial phase transformation experiment on a Fe-0.1C-1.0Mn alloy close to the inversion stage at which the interface migrates at a rather low velocity. The low velocity allowed capturing the interface pinning effect over a period of no less than 16 seconds. From our observations, it was possible to follow the progression of the pinning effect from the initial stages all the way through to the release of the interface. The pinning force exerted by the individual particle having a diameter of 140 nm on the austenite-ferrite interface was estimated as 175 nJ m−1, while the maximum pinning length was approximately 750 nm to either side of the particle, leading to an interface line tension of 170 nJ m−1. The observed pinning behavior is compared with the most relevant models in the literature.@en