Metal additive manufacturing (AM) by Laser-Directed Energy Deposition (L-DED) usually results in the formation of textured columnar grains along the build direction, leading to anisotropic mechanical properties. This can negatively affect the intended application of the product. Anisotropy can be eliminated by modifying the material through an additional exposure to ultrasound (US-assisted) during the L-DED process. In this paper, a multi-track sample was manufactured from AISI H13 (TLS Technik, Bitterfeld-Wolfen, Germany) tool steel by a US-assisted (28 kHz) L-DED process using a specially designed cooling system. The study also included post-process annealing and quenching with the tempering heat treatment of the modified steel, resulting in the retention of the properties, as confirmed by hardness measurements. XRD analysis was used to measure the structural parameters of the unit cell, and the hardness properties were measured in two directions: longitudinally and parallel to the deposition direction. It was found that US-assisted L-DED allows us to obtain a more isotropic structure with an equal size of the coherent scattering region in two printing directions, and to reduce the residual stresses in the material. The anisotropy of the hardness was significantly reduced, with 636 and 640 HV found between the XY and XZ planes. Based on the obtained hardness data, it should be noted that some of the heat treatments studied herein can also result in a decrease in the anisotropy of the properties, similarly to the US-assisted effect.

In this study, bulk samples of a CrMoNbWV high-entropy alloy (HEA) were obtained for the first time by spark plasma sintering (SPS) of mechanically alloyed (MA) powders at 1200 °C, 1300 °C, and 1400 °C. Microstructure evolution, phase formation as well as wear and corrosion behavior were investigated. The MA powders’ phase composition was found to be represented by body-centered-cubic (BCC) solid solution. The solid solution partially decomposed to Laves phases under the sintering, such as Cr2Nb and (Fe, Cr)Nb, and NbVO4-VO oxides mixture. The temperature increase to 1400 °C led to a grain coarsening of the BCC phase and decreased the Laves phase content accompanied by precipitation at the grain boundaries. The sintered samples showed high hardness and compressive strength (2700–2800 MPa) at room temperature. The wear tests demonstrated excellent results in comparison to conventional wear-resistant composites. The obtained samples also exhibited high corrosion resistance under electrochemical tests in H2SO4 solution. The CrMoNbWV HEA has comparable mechanical and corrosive properties with the WNbMoTaV type HEA, but at the same time has a reduced density: CrMoNbWV—10.55 g/cm3, WNbMoTaV—12.42 g/cm3

The aim of this study was to determine the influence of heat treatment on the microstructure of single-crystal nickel-based alloy manufactured by selective laser melting with a high-temperature substrate preheating. The change of gamma/gamma prime -phases ratio was established as a result of various heat treatment modes.

16Cr-2Ni-Mn-Mo-xN (wt%) stainless steel powders were synthesized by mechanical alloying from elemental metal and chromium nitride (Cr2N) powders. Compaction of resulting powders was carried out using spark plasma sintering technology. The X-Ray diffraction and Scanning Electron Microscopy analysis showed that chemical homogeneity improves with increasing alloying time and decreasing nitrides powder content. Analysis of sintering samples showed the formation of a and ?-phase solid solution with nitrogen-containing samples containing undissolved nitrogen inclusions. The results of high-temperature tensile tests showed an increase of tensile stress for the sample containing 50% Cr2N. Furthermore, the microhardness was increased with an increase in the amount of Cr2N.