Time-resolved X-ray study of assisted fluidization of cohesive micron powder
On the role of mechanical vibration
K. Wu (TU Delft - ChemE/Product and Process Engineering)
E. C. Wagner (TU Delft - ChemE/O&O groep)
Olga Ochkin-Koenig (BASF SE)
Miika Franck (BASF SE)
Dominik Weis (BASF SE)
Gabrie M.H. Meesters (TU Delft - ChemE/Product and Process Engineering)
J. R. Van Ommen (TU Delft - ChemE/Product and Process Engineering)
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Abstract
Mechanical vibration has been broadly used to assist fluidization of cohesive powders, because of its capability to disrupt gas channels and agglomerates. However, the improvement reported in literature is mostly deduced from bulk response and ex-situ measurements, whereas the induced fluidization behavior and underlying physics remain largely unexplored. In this work, the fluidization behavior of micron-sized cohesive silica (Sauter mean diameter D32 = 7.9 μm) has been investigated experimentally under vibration of varying conditions. X-ray imaging was carried out to directly capture the temporal evolution of system hydrodynamics, and identify in-situ powder stratification, bubbling and channel formation. The study demonstrates that vibration effectively collapses gas channels, yet facilitates powder stratification and compaction, therefore developing three distinctive flow regions inside the bed with different fluidization states. Consequently, common measurements, such as pressure drop and bed expansion, tend to overestimate the improvement. In addition, increasing frequency, from 10 Hz to 30 Hz, is observed to increase the number of bubbles by 60 %, whereas a large amplitude (e.g., 2 mm) leads to a 10 % compaction in the top flow region.
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