Micro-mechanical properties of alkali-activated fly ash evaluated by nanoindentation

Journal article (2017)

Authors

Y. Ma Guangzhou University

G. Ye Materials and Environment - , Universiteit Gent

J Hu South China University of Technology

Research Group

Materials and Environment () (TU Delft)

Nanoindentation Elastic modulus Alkali-activated fly ash

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http://resolver.tudelft.nl/uuid:de479139-4531-423c-b8cd-061d75e31aa7

Published Date

30-08-2017

Language

English

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Faculty

Civil Engineering & Geosciences

Department

Materials- Mechanics- Management & Design

Research Group

Materials and Environment

Abstract

In this study, the micro-mechanical property of different phases in alkali-activated fly ash (AAFA) pastes was investigated by nanoindentation. The mechanical information of the gel phase in AAFA was then linked to the chemical and microstructural information provided by SEM-EDX, ATR-FTIR and N₂ adsorption, respectively. Three phases, i.e. aluminosilicate gel, residual fly ash particles and pores, were identified from the microstructural analysis of AAFA, corresponding to three distinct peaks in the indentation modulus frequency plots. The peak corresponding to the gel phase varied with curing age and activator content. The elastic modulus of aluminosilicate gel measured by nanoindentation was affected by the pores between nano to micro scale. The results of the chemical bonds of AAFA, however, cannot correspond well with the micromechanical results.

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