Print Email Facebook Twitter Local changes in the microstructure, mechanical and electrochemical properties of friction stir welded joints from aluminium of varying grain size Title Local changes in the microstructure, mechanical and electrochemical properties of friction stir welded joints from aluminium of varying grain size Author Orłowska, Marta (Military University of Technology) Pixner, Florian (Graz University of Technology) Hütter, Andreas (Graz University of Technology) Kooijman, A.M. (TU Delft Team Arjan Mol) Jasiński, Cezary (Warsaw University of Technology) Gonzalez Garcia, Y. (TU Delft Team Yaiza Gonzalez Garcia) Enzinger, Norbert (Graz University of Technology) Lewandowska, Małgorzata (Warsaw University of Technology) Date 2021 Abstract The present study shows results of friction stir welded (FSW) samples after different plastic deformation routes. The welds were made of coarse-grained and ultrafine-grained commercially pure aluminium. As a plastic deformation method a new hybrid process has been chosen, which resulted in obtaining samples with different characteristics of microstructure, which also differed in dependance of the examined plane. Microstructure observations showed that, regardless of the base material, due to continuous dynamic recrystallization a stir zone was characterized by equiaxial grains with an average size of 3.5–5.0 μm. However, significant differences in the changes of the microstructure in thermomechanically affected and heat affected zones have been obtained between welds. Microhardness profiles revealed a decrease in the stir zones in comparison with the initially deformed samples, but an increase for the annealed samples. Tensile tests showed differences between the samples. In the deformed samples, the rupture occurred in a stir zone, while in the undeformed samples in the base material. In addition, due to the application of 3D digital image correlation, it was possible to observe deformation and local changes between the weld zones during the tensile test. Additionally, local electrochemical measurements were performed with two sizes of working electrode, which included the application of microcapillary technique. The results showed higher corrosion resistance in 3.5% NaCl in the stir zones. Subject AluminiumFriction stir weldingLocal characterizationMechanical propertiesMicrocapillaryUltrafine-grained microstructure To reference this document use: http://resolver.tudelft.nl/uuid:eba06ba0-fffd-4264-a4fb-06e1448ba6ed DOI https://doi.org/10.1016/j.jmrt.2021.11.057 ISSN 2238-7854 Source Journal of Materials Research and Technology, 15, 5968-5987 Part of collection Institutional Repository Document type journal article Rights © 2021 Marta Orłowska, Florian Pixner, Andreas Hütter, A.M. Kooijman, Cezary Jasiński, Y. Gonzalez Garcia, Norbert Enzinger, Małgorzata Lewandowska Files PDF 1_s2.0_S2238785421013375_main_1.pdf 10.6 MB Close viewer /islandora/object/uuid:eba06ba0-fffd-4264-a4fb-06e1448ba6ed/datastream/OBJ/view