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Van Landschoot, N. (author)Chapter 2 describes the solid-state synthesis of LiNiVO4 and LiCoVO4. The materials are prepared at 800C and are phase pure, as shown by X-ray diffraction and have the inverse spinel structure. Due to the solid-state synthesis the particle size is quite large and the particle size distribution is large, between 0.1mm and 10 mm, even after ball...doctoral thesis 2006