Selective oxidation of aluminium in Mo(Al,Si)₂

Mo(Al_xSi_1-x)₂ alloy with x in the range of 0.35–0.65 were prepared by a one-step spark plasma sintering. To study the exclusive formation of an α-Al₂O₃ scale, oxidation experiments were conducted in low and high oxygen partial pressure ambient at 1373 K; viz.: 10⁻¹⁴ and 0.21...

Effects of boron addition on the high temperature oxidation of MoSi₂ alloys

Boron containing MoSi₂ is a promising material for applications at high temperature, but the oxidation mechanism is still unclear. In this work, the high temperature (1100 °C) oxidation of B doped MoSi₂ in synthetic air has been investigated. A (boro)silicate layer is formed on the surface of the alloy, which features a...

Healing cracks in additively manufactured NiTi shape memory alloys

The pursuit of enhancing NiTi superelasticity through laser powder bed fusion (L-PBF) and [001] texture creation poses a challenge due to increased susceptibility to hot cracking in the resulting microstructure with columnar grains. This limitation restricts NiTi's application and contributes to material waste. To overcome this, we introduce...

Mo(Al_xSi_1−x)₂ healing particles for high temperature ceramics and encapsulation by selective oxidation of aluminium

To prevent premature triggering of the healing reaction in Mo-Si containing self-healing thermal barrier coating system, an oxygen impenetrable shell (α-Al₂O₃) around the sacrificial healing particles (MoSi₂) is desired. Here an encapsulation method is presented through selective oxidation of Al in Mo(Al<sub>x...

Applicability study of pulsed laser beam welding on ferritic–martensitic ODS eurofer steel

Pulsed laser beam welding was used successfully to join the oxide dispersion-strengthened (ODS) Eurofer steel. The joining was conducted with a laser power of 2500 W and a pulsed duration of 4 ms. With the filler material being used, a minor material loss and microvoids were observed in the joint. The microstructure of the fusion zone...

Microstructure characterisation and mechanical properties of ODS Eurofer steel subject to designed heat treatments

The present work deals with oxide dispersion strengthened (ODS) Eurofer steel fabricated by powder metallurgy involving mechanical alloying and spark plasma sintering. A heat treatment route including normalising and tempering was applied to the as-produced steel, based on differential scanning calorimetry (DSC) measurement. The...

Solid State Diffusion Bonding of ODS Eurofer Steel by Spark Plasma Sintering

Oxide dispersion strengthened (ODS) steels are considered to be one of the candidate structural materials for advanced nuclear applications due to their high elevated-temperature strength, corrosion resistance, and radiation tolerance. Joining of ODS steels by traditional fusion joining techniques is not applicable, because the melting...

Effect of mechanical alloying and spark plasma sintering on the microstructure and mechanical properties of ODS Eurofer

Oxide dispersion strengthened (ODS)Eurofer steel was prepared via mechanical alloying (MA)and spark plasma sintering (SPS). Different combinations of MA and SPS parameters were adopted in order to optimise the fabrication process. The experimental results show that the sample milled for 30 h, sintered at 1373 K at a pressure of 60 MPa has...