Microstructural stability of secondary phases in an ODS ferritic steel after thermal aging at 873 K

An oxide dispersion strengthened (ODS) steel with nominal composition Fe–14Cr–2W–0.4Ti–0.3Y₂O₃ (wt%) has been manufactured by mechanical alloying of pre-alloyed powders with nanosized Y₂O₃, compacted by hot isostatic pressing and hot cross rolled. In order to evaluate the long-term thermal...

Achieving superelasticity in additively manufactured Ni-lean NiTi by crystallographic design

Superelastic metallic materials possessing large recoverable strains are widely used in automotive, aerospace and energy conversion industries. Superelastic materials working at high temperatures and with a wide temperature range are increasingly required for demanding applications. Until recently, high-temperature superelasticity has only...

Dislocations, texture and stress development in hydrogen-cycled Pd thin films: An in-situ X-ray diffraction study

For Pd thin films, microstructural changes involved during hydrogen cycling provide the information needed to predict and optimize the film's mechanical strength. In this paper, a systematic study of the morphology, microstructure, texture, and stress has been performed on Pd thin films during hydrogen loading and deloading cycles at room...

Controlling microstructure evolution and phase transformation behavior in additive manufacturing of nitinol shape memory alloys by tuning hatch distance

Laser powder bed fusion (L-PBF), categorized as additive manufacturing technique, has a capability to fabricate NiTi (Nitinol) shape memory alloys with tailorable functional properties and complex geometries. An important processing parameter, hatch distance (h), is often related to macroscale structural defects; however, its role on...

Effect of Sr Addition to a Modified AA3003 on Microstructural and Corrosion Properties

Sr is known to transform the morphology of the eutectic silicon phase as well as the Fe-rich β phase in Al-Si alloys, improving their mechanical properties. However, little is known about the effect Sr has on the (local) corrosion properties of aluminium alloys. This study investigates the effect of Sr addition to a modified AA3003 heat...

Interplay between metastable phases controls strength and ductility in steels

By means of high-energy synchrotron X-ray diffraction, the interplay between martensite and retained austenite phases in steel during the application of stress has been analyzed. Martensite properties were varied through controlled reheating heat treatments in a low carbon Quenched and Partitioned (Q&P) steel consisting of retained...

Residual stress measurements and model validation of single and double pulse resistance spot welded advanced high strength steel

Advanced high strength steels (AHSS) are increasingly used in automotive industry; thousands of resistance spot welds are applied to car body-in-white. High alloying levels of AHSS result in lower weldability. Residual stresses play an essential role on the formation of defects and the mechanical performance of the weld. An electrical-thermal...

In-situ synchrotron X-ray diffraction studies on effects of plastic and Eelastic loading on bcc phase transformations of a 3rd generation 1 GPa advanced high strength steel

In this paper, we describe the effects of mechanical loading on bcc-to-bcc phase transformations of an Advanced High Strength Steel during cooling. In-situ synchrotron diffraction was employed to measure time–temperature–load diffraction patterns. Calculations were made of the volume fractions of the phases, the transformation kinetics, and...

Controlling the work hardening of martensite to increase the strength/ductility balance in quenched and partitioned steels

The role of retained austenite on tensile behavior in quenched and partitioned (Q&P) steels has been studied extensively, but the deformation behavior of martensite, which comprises the majority of Q&P microstructures, has received less attention. In this investigation, martensite properties were varied through heat treatment in a low...

High-resolution X-ray diffraction investigation on the evolution of the substructure of individual austenite grains in TRIP steels during tensile deformation

The martensitic transformation behaviour of the metastable austenite phase in low-alloyed transformation-induced plasticity (TRIP) steels has been studied in situ using high-energy X-ray diffraction during deformation. The austenite stability during tensile deformation has been evaluated at different length scales. A powder diffraction analysis...