Carbon fiber-reinforced polymers (CFRPs) have widely attracted the aerospace and automotive industries due to high stiffness and lightweight. Secondary adhesive bonding of CFRPs is a promising research field to fully explore their potential. However, multiple challenges have limited the further application of adhesively-bonded composite joints since it is difficult to inspect the premature debonding, which leads to catastrophic failure once initiated. Thus, it is crucial to introduce crack arrest features, to slow down (or even stop) the crack growth and achieve progressive failure. Various methods have been reported to introduce crack arrest features, including z-pins and corrugated substrates. Our previous work directly utilized the adhesive layer to bridge the separating CFRP parts, through the extrinsic bridging of adhesive ligaments. The bridging adhesive ligaments are triggered by the patterning of distinct surface treatments. These extrinsic bridging ligaments largely enhance the energy release rate (ERR) and successfully arrest the crack propagation. However, a large portion of the required energy for the further crack propagation is stored elastically in the stretching ligaments, which would cause catastrophic fast joint debonding after the failure of ligaments. In this work, the adhesive layer was architected in order to improve its plasticity. By promoting the plastic energy dissipation, the bridging, stretching, and failure of generated adhesive ligaments could result in tougher and safer joints. CFRP substrates were alternatively patterned by two distinct surface treatments to achieve different interfacial strength and toughness values. Then, double-cantilever beams (DCB) were manufactured by bonding treated substrates with the architected adhesive material, such as integrating 3D-printed nylon wires or newly synthesized adhesive material. Results showed that the proposed joint toughening strategy could improve ERR compared to conventional uniform treatments and increasd adhesive plasticity could also stabilize the crack propagation, leading to a safer joint. @en

Damage initiation and evolution of three-dimensional (3D) orthogonal woven carbon fibre composite (3DOWC) is investigated experimentally and numerically. Meso-scale homogenisation of the representative volume element (RVE) is utilised to predict the elastic properties, simulate damage initiation and evolution when loaded in tension. The effect of intra-yarns transverse cracking and shear diffused damage on the in-plane transverse modulus and shear modulus is investigated while one failure criterion is introduced to simulate the matrix damage. The proposed model relies on two major assumptions. First, the effect of the binder yarns, on the in-plane properties, is neglected, so the 3DOWC unit cell can be approximated as a (0°/90°) cross-ply laminate. Second, a micro-mechanics based damage approach is used at the meso-scale, so damage indicators can be correlated, explicitly, to the density of cracks within the material. Results from the simulated RVE are validated against experimental results along the warp (0° direction) and weft (90° direction). This approach paves the road for more predictive models as damage evolution laws are obtained from micro mechanical considerations and rely on few well-defined material parameters. This largely differs from classical damage mechanics approaches in which the evolution law is obtained by retrofitting experimental observations.@en

Damage initiation and evolution of three-dimensional (3D) orthogonal woven carbon fibre composite (3DOWC) is investigated experimentally and numerically. Meso-scale homogenisation of the representative volume element (RVE) is utilised to predict the elastic properties, simulate damage initiation and evolution when loaded in tension. The effect of intra-yarns transverse cracking and shear diffused damage on the in-plane transverse modulus and shear modulus is investigated while one failure criterion is introduced to simulate the matrix damage. The proposed model relies on two major assumptions. First, the effect of the binder yarns, on the in-plane properties, is neglected, so the 3DOWC unit cell can be approximated as a (0°/90°) cross-ply laminate. Second, a micro-mechanics based damage approach is used at the meso-scale, so damage indicators can be correlated, explicitly, to the density of cracks within the material. Results from the simulated RVE are validated against experimental results along the warp (0° direction) and weft (90° direction). This approach paves the road for more predictive models as damage evolution laws are obtained from micro mechanical considerations and rely on few well-defined material parameters. This largely differs from classical damage mechanics approaches in which the evolution law is obtained by retrofitting experimental observations.@en

Damage initiation and evolution of three-dimensional (3D) orthogonal woven carbon fibre composite (3DOWC) is investigated experimentally and numerically. Meso-scale homogenisation of the representative volume element (RVE) is utilised to predict the elastic properties, simulate damage initiation and evolution when loaded in tension. The effect of intra-yarns transverse cracking and shear diffused damage on the in-plane transverse modulus and shear modulus is investigated while one failure criterion is introduced to simulate the matrix damage. The proposed model relies on two major assumptions. First, the effect of the binder yarns, on the in-plane properties, is neglected, so the 3DOWC unit cell can be approximated as a (0°/90°) cross-ply laminate. Second, a micro-mechanics based damage approach is used at the meso-scale, so damage indicators can be correlated, explicitly, to the density of cracks within the material. Results from the simulated RVE are validated against experimental results along the warp (0° direction) and weft (90° direction). This approach paves the road for more predictive models as damage evolution laws are obtained from micro mechanical considerations and rely on few well-defined material parameters. This largely differs from classical damage mechanics approaches in which the evolution law is obtained by retrofitting experimental observations.@en

Electrical resistance monitoring (ERM) has been used to study the effect of the z-binding yarns on the initial electrical resistance (ER) and its change of three architectures of 3D woven carbon fibre composites namely (orthogonal “ORT”, layer-to-layer “LTL” and angle interlock “AI”) when tested in tension. Specimens are loaded in on-axis “warp” and off-axis “45°” directions. In situ ERM is achieved using the four-probe technique. Monotonic and cyclic “load/unload” tests are performed to investigate the effect of piezo-resistivity and residual plasticity on resistance variation. The resistance increase for the off-axis loaded specimens (∼90%) is found to be higher than that of their on-axis counterparts (∼20%). In the case of cyclic testing, the resistance increase upon unloading is irreversible which suggests permanent damage presence not piezo-resistive effect. At the moment, it is difficult to obtain a direct correlation between resistance variation and damage in 3D woven composites due to the complexity of the conduction path along the three orthogonal directions, however this study demonstrates the potential of using ERM for damage detection in 3D woven carbon fibre-based composites and highlights the challenges that need to be overcome to establish ERM asa Structural Health Monitoring (SHM) technique for such material systems.@en

Electrical resistance monitoring (ERM) has been used to study the effect of the z-binding yarns on the initial electrical resistance (ER) and its change of three architectures of 3D woven carbon fibre composites namely (orthogonal “ORT”, layer-to-layer “LTL” and angle interlock “AI”) when tested in tension. Specimens are loaded in on-axis “warp” and off-axis “45°” directions. In situ ERM is achieved using the four-probe technique. Monotonic and cyclic “load/unload” tests are performed to investigate the effect of piezo-resistivity and residual plasticity on resistance variation. The resistance increase for the off-axis loaded specimens (∼90%) is found to be higher than that of their on-axis counterparts (∼20%). In the case of cyclic testing, the resistance increase upon unloading is irreversible which suggests permanent damage presence not piezo-resistive effect. At the moment, it is difficult to obtain a direct correlation between resistance variation and damage in 3D woven composites due to the complexity of the conduction path along the three orthogonal directions, however this study demonstrates the potential of using ERM for damage detection in 3D woven carbon fibre-based composites and highlights the challenges that need to be overcome to establish ERM asa Structural Health Monitoring (SHM) technique for such material systems.@en

Three different architectures of 3D carbon fibre woven composites (orthogonal, ORT; layer-to-layer, LTL; angle interlock, AI) were tested in quasi-static uniaxial tension. Mechanical tests (tensile in on-axis of warp and weft directions as well as 45° off-axis) were carried out with the aim to study the loading direction sensitivity of these 3D woven composites. The z-binder architecture (the through-thickness reinforcement) has an effect on void content, directional fibre volume fraction, mechanical properties (on-axis and off-axis), failure mechanisms, energy absorption and fibre rotation angle in off-axis tested specimens. Out of all the examined architectures, 3D orthogonal woven composites (ORT) demonstrated a superior behaviour, especially when they were tested in 45° off-axis direction, indicated by high strain to failure (∼23%) and high translaminar energy absorption (∼40MJ/m3). The z-binder yarns in ORT architecture suppress the localised damage and allow larger fibre rotation during the fibre “scissoring motion” that enables further strain to be sustained by the in-plane fabric layers during off-axis loading.@en

Degradation from mechanical loading of transparent electrodes made of indium tin oxide (ITO) endangers the integrity of any material based on these electrodes, including flexible organic solar cells. However, how different schemes of degradation change the conductivity of ITO devices remains unclear. We propose a systematic micro-mechanics-based approach to clarify the relationship between degradation and changes in electrical resistance. By comparing experimentally measured channel crack densities to changes in electrical resistance returned by the different micro-mechanical schemes, we highlight the key role played by the residual conductivity in the interface between the ITO electrode and its substrate after delamination. We demonstrate that channel cracking alone does not explain the experimental observations. Our results indicate that delamination has to take place between the ITO electrode and the substrate layers and that the residual conductivity of this delaminated interface plays a major role in changes in electrical resistance of the degraded device.@en

The effect of circular notch has been evaluated for three different architectures of three-dimensional (3D) carbon fibre woven composites (orthogonal, ORT; layer-to-layer, LTL; angle interlock, AI) through open-hole quasi-static tension and double-lap bearing strength tests in the off-axis (45textdegree) direction. Damage characterisation is monitored using Digital Image correlation (DIC) for open-hole testing and X-ray Computed Tomography (CT) for double-lap bearing strength test. The off-axis notched 3D woven composites exhibits minor reduction (less than 10 %) of the notched strength compared to the un-notched strength. DIC strain contour clearly show stress/strain localisation regions around the hole periphery and stress/strain redistribution away from the whole due to the z-binder existence, especially for ORT architecture. Up to 50 % bearing strain, no significant difference in the bearing stress/bearing strain response is observed. However when ORT architecture was loaded up to failure, it demonstrates higher strain to failure (textasciitilde140 %) followed by AI (textasciitilde105 %) and lastly LTL (textasciitilde85 %). X-ray CT scans reveal the effect of the z-binder architecture on damage evolution and delamination resistance. The study suggests that off-axis loaded 3D woven composites, especially ORT architecture, has a great potential of overcoming the current challenges facing composite laminates when used in composite joints' applications.@en