This study presents a new method with improved accuracy for measuring the tensile properties of elementary flax fibres using an automated single-fibre tester with Digital Image Correlation (DIC) for strain tracking, validated with glass fibres of known properties. Modulus values were obtained for glass fibres (83±5.17 GPa, 12mmGL; 79.4±1.33 GPa, MidFibre) and elementary flax fibres (77.0±15.3 GPa, 12mmGL; 74.8±20.2 GPa, MidFibre) using speckle patterns on both end tabs and on optical flags attached to the fibres. This study highlights the advantages of automated single-fibre testing and optical extensometry for reliable and efficient measurement of tensile properties of single fibres.

As a sustainable and eco-friendly material, flax fibres offer a viable alternative to glass fibres in composite applications due to their good specific mechanical properties. However, addressing their moisture sensitivity is crucial to expanding their use in various applications. This study investigates the impact of enzymatic treatment on improving the moisture resistance of flax fibres. FlaxTapeTM 200 was treated with two types of polygalacturonase enzymes to selectively remove pectin. The moisture resistance of the treated fibres and their composites was compared with that of untreated samples. The results revealed a significant reduction in moisture uptake at high relative humidity conditions and a decrease in percentage water uptake in both longitudinal and transverse composites after enzymatic treatment. FTIR spectra and contact angle measurement results supported the observed improvement in the moisture resistance of flax fibres. This study highlights the effectiveness of enzymatic treatment in enhancing the moisture durability of flax fibres which further broadens their potential for structural and lightweight composite materials.

The aim of this study was to determine the effect of moisture cycling (environmental relative humidity cycles) on the durability of flax-epoxy composites and investigate the influence of cycling duration and temperature on the stiffening and strengthening of flax fibres. Four moisture cycling protocols for flax fibres were employed in this research which includes 4D21 (4days per cycle at 21ºC), 4D60 (4days per cycle at 60ºC), 3H27 (3hours per cycle at 27ºC) and 3H60 (3hours per cycle at 60ºC). To measure the impact of high-low humidity cycling at different cycling durations and temperature, tensile testing of impregnated fibre bundle test (IFBT) samples was done. Results of the back-calculated properties revealed that the applied cycling protocols enhanced both the tensile strength and modulus of the fibres. Better improvement of tensile properties was observed in fibres cycled at longer duration. The fibres undergoing 4 days of cycling at 21ºC (4D21 fibres) showed the highest improvements in tensile strength (18%), as well as tensile moduli E1 (19%) and E2 (18%) after 10 cycles. Interestingly, all fibres showed increased stiffness (E1) in the range of 8-20% after 10 cycles and 4-8% after 20 cycles. This fibreimprovement in mechanical strength and stiffness of the fibres can possibly be attributed to a phenomenon similar to a hornification effect in wood or possibly by fibre repair due to pectin migration, which produces the strengthening and stiffening effect.