Phase-transformation and precipitation kinetics in vanadium micro-alloyed steels by in-situ, simultaneous neutron diffraction and SANS

In-situ Neutron Diffraction and Small-Angle Neutron Scattering (SANS) are employed for the first time simultaneously in order to reveal the interaction between the austenite to ferrite phase transformation and the precipitation kinetics during isothermal annealing at 650 and at 700 °C in three steels with different vanadium (V) and carbon (C)...

Evolution of the precipitate composition during annealing of vanadium micro-alloyed steels by in-situ SANS

In-situ Small-Angle Neutron Scattering (SANS) is used to determine the time evolution of the chemical composition of precipitates at 650 °C and 700 °C in three micro-alloyed steels with different vanadium (V) and carbon (C) concentrations. Precipitates with a distribution of substoichiometric carbon-to-metal ratios are measured in all steels....

Interaction of precipitation with austenite-to-ferrite phase transformation in vanadium micro-alloyed steels

The precipitation kinetics of vanadium carbides and its interaction with the austenite-to-ferrite phase transformation is studied in two micro-alloyed steels that differ in vanadium and carbon concentrations by a factor of two, but have the same vanadium-to-carbon atomic ratio of 1:1. Dilatometry is used for heat-treating the specimens and...

1.5 GPa compact double-wall clamp cell for SANS and NSE studies at low temperatures and high magnetic fields

We have developed and realised a compact high-pressure clamp cell of the piston-cylinder type for Small Angle Neutron Scattering (SANS) and Neutron Spin Echo (NSE) spectroscopy measurements. The cell can pressurise φ5 mm samples up to 1.5 GPa. It is non-magnetic, produces a sufficiently low and flat SANS background with a relatively good...