V.P. Perruchoud
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9 records found
1
This study investigates unidirectional flax fibre composites with epoxy (EP) and partially bio-based unsaturated polyester (UP) matrices conditioned to three humidity conditions (20%RH, 50%RH, and 85%RH) to assess how the resin system influences mechanical performance under hygroscopic exposure. Specimens were subjected to quasi-static tension, flexion, and tension-tension fatigue. Moisture uptake was observed to strongly influence both the quasi-static and fatigue behaviour of the flax fibre composites. Increasing the relative humidity from 20% to 85% led to a reduction in both tensile and flexural modulus, with decreases of approximately 12% for EP-Flax and about 24% for UP-Flax. The modulus measured during fatigue decreased by approximately 25% for both composites with increasing humidity. The effect of humidity on fatigue life depended on the matrix system, with EP-Flax exhibiting greater fatigue resistance than UP-Flax. Increasing humidity also increased hysteresis energy, loss factor and residual strain, indicating greater irreversible deformation. Interrupted cross-sectional microscopy revealed earlier fibre-bundle cracking in UP-Flax and a humidity-dependent shift towards cracking within individual fibres. Post-fatigue fibre pull-out also increased with humidity, indicating reduced interfacial resistance. These apparently competing effects suggest that, in the fibre-dominated EP-Flax laminates, increased deformation capacity and stress redistribution can delay final failure despite partial interfacial degradation.
FRP structures are subjected to a combination of environmental and mechanical loads that act in an interactive way, determining service life. This study investigates the isolated and combined effects of in-situ temperature and relative humidity on monotonic and tension-tension fatigue response of two flax/epoxy laminates ([0/90/0]S and [+45/-45]2S), benchmarked against equivalent GFRP laminates. Particular emphasis was given to stiffness evolution, strain accumulation, and hysteretic behaviour particularly energy dissipation. Increasing temperature consistently reduced stiffness, strength, and fatigue life for both flax FRP laminates, leading to downward shifts and tilts of the S–N curves. The effect of moisture alone was laminate-dependent: elevated moisture content reduced stiffness, strength and fatigue life in the shear-dominated [+45/-45]2S laminate, whereas the [0/90/0]S laminate showed increased fatigue life attributed to enhanced ductility and increased laminate strength. Combined elevated temperature and moisture content lead to reduced monotonic stiffness and strength whilst their effects on fatigue life were cumulative. The largest effect was observed for the [+45/-45]2S laminate, where fatigue life decreased by approximately three orders of magnitude. Across all hygrothermal conditions, energy dissipation was found to be an indicator of fatigue life with higher hysteretic energy dissipation per cycle correlated with reduced fatigue life. When assessed relative to baseline S–N behaviour, flax FRPs exhibit a proportional sensitivity to combined temperature and humidity comparable to GFRPs, indicating that flax composites are not disproportionately penalised under hot–wet fatigue loading.
Therefore, this study proposes a novel methodology to estimate fatigue energy dissipation in FRP composites using only monotonic test data. The approach introduces the total work ratio (RW,tot), defined as the ratio between the cumulative dissipated work and the cumulative applied work over the fatigue life. Provided the applied work can be determined, based on material stiffness and loading parameters, RW,tot enables estimation of fatigue energy dissipation. Because the method is grounded in monotonic experiments, it inherently captures material-specific dissipative mechanisms.
The methodology is validated through experimental testing on a [0/90/0] glass FRP laminate and two flax fibre-reinforced biocomposite laminates: [0/90/0]S and [(+45/−45)2]S. Fatigue results indicate a linear dependence of RW,tot on the applied stress level that interestingly align with monotonic results. For the [0/90/0]S flax composite, this linear relationship intersects the origin, allowing direct estimation of RW,tot in fatigue solely from monotonic data under matched strain rates. In contrast, the [(+45/−45)2]S laminate does not exhibit origin-crossing linearity, potentially due to time-dependent mechanisms such as viscoelastic creep.
While further investigation is required to generalise the method across diverse laminate architectures, the findings highlight a simple, experimentally grounded, and physically interpretable approach for estimating energy dissipation in fatigue of FRP composites, potentially enabling more efficient fatigue life prediction.
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Therefore, this study proposes a novel methodology to estimate fatigue energy dissipation in FRP composites using only monotonic test data. The approach introduces the total work ratio (RW,tot), defined as the ratio between the cumulative dissipated work and the cumulative applied work over the fatigue life. Provided the applied work can be determined, based on material stiffness and loading parameters, RW,tot enables estimation of fatigue energy dissipation. Because the method is grounded in monotonic experiments, it inherently captures material-specific dissipative mechanisms.
The methodology is validated through experimental testing on a [0/90/0] glass FRP laminate and two flax fibre-reinforced biocomposite laminates: [0/90/0]S and [(+45/−45)2]S. Fatigue results indicate a linear dependence of RW,tot on the applied stress level that interestingly align with monotonic results. For the [0/90/0]S flax composite, this linear relationship intersects the origin, allowing direct estimation of RW,tot in fatigue solely from monotonic data under matched strain rates. In contrast, the [(+45/−45)2]S laminate does not exhibit origin-crossing linearity, potentially due to time-dependent mechanisms such as viscoelastic creep.
While further investigation is required to generalise the method across diverse laminate architectures, the findings highlight a simple, experimentally grounded, and physically interpretable approach for estimating energy dissipation in fatigue of FRP composites, potentially enabling more efficient fatigue life prediction.
Additionally, the pre-creeping and fatigue interruptions were found to substantially impact fatigue life, particularly in laminates with yarn twist, leading to a 1.7-fold increase due to interruptions and a threefold increase following pre-creeping. The latter also yielding a near-elimination of strain accumulation. Therefore, pre-creeping is proposed as an effective strategy to reduce in-service strain accumulation and extend fatigue life in predominantly UD flax FRPs with twisted yarns. ...
Additionally, the pre-creeping and fatigue interruptions were found to substantially impact fatigue life, particularly in laminates with yarn twist, leading to a 1.7-fold increase due to interruptions and a threefold increase following pre-creeping. The latter also yielding a near-elimination of strain accumulation. Therefore, pre-creeping is proposed as an effective strategy to reduce in-service strain accumulation and extend fatigue life in predominantly UD flax FRPs with twisted yarns.
Hygrothermal Fatigue of Structural Biocomposites
Pathways to Damage Analysis and Lifetime Prediction
A concept is proposed to relate the hygrothermal fatigue behaviour of biobased FRP composites to their fatigue behaviour in standard laboratory air conditions, using damage analysis comprised of permanent strains and stiffness variations measurements, as well as visual macro and micro damage inspections, to enable the development of a mechanism based lifetime predictions model.
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A concept is proposed to relate the hygrothermal fatigue behaviour of biobased FRP composites to their fatigue behaviour in standard laboratory air conditions, using damage analysis comprised of permanent strains and stiffness variations measurements, as well as visual macro and micro damage inspections, to enable the development of a mechanism based lifetime predictions model.