T. Bristogianni
Please Note
10 records found
1
Thermal Treatment as a Repair Method for Naturally Weathered Aged Glass
An Experimental Study on Surface Flaws, Fracture Strength, and Strength Prediction
Specimens were obtained from approximately 42-year-old insulating glass units and tested in an untreated condition or after thermal treatment at 500°C, 540°C, or 600°C. Surface damage was characterized using optical microscopy, image analysis, and laser line scanning. Surface prestress was measured using a SCALP-05 device, while fracture strength was determined through coaxial double ring testing and evaluated using Weibull statistics. Finite element modeling was used to verify the stress distribution during testing, and Linear Elastic Fracture Mechanics was considered for predicting strength from measured flaw dimensions.
Microscopy and image analysis did not provide conclusive evidence of visible flaw healing after thermal treatment. Most scratches and defects remained detectable, while treatment at 600°C produced bubble-like features on some specimens. The mechanical results showed that the effect of thermal treatment depended on both temperature and the loaded glass surface. For the air side, thermal treatment did not consistently improve the lower-tail strength. For the tin side, treatment at 540°C produced the greatest improvement at low failure probabilities, increasing the failure strength by 33.2% at a failure probability of 0.8% and by 23.1% at 5%. Although treatment at 600°C resulted in a greater increase in median strength, it slightly reduced the strength at the lowest failure probability and introduced additional surface defects.
The laser line scanner was unsuitable for reliable characterization of strength-governing flaws because of transparency, reflectivity, scanning-spray effects, and insufficient spatial and vertical resolution. Consequently, fracture strength could not be reliably predicted from the measured flaw dimensions.
Overall, thermal treatment at approximately 540°C showed the most promising balance between improving the structural reliability of naturally weathered glass and avoiding additional material damage. However, the strength improvement could not be directly related to visible flaw healing, and the investigated non-destructive methods were insufficient for predicting the strength of individual panes. ...
Specimens were obtained from approximately 42-year-old insulating glass units and tested in an untreated condition or after thermal treatment at 500°C, 540°C, or 600°C. Surface damage was characterized using optical microscopy, image analysis, and laser line scanning. Surface prestress was measured using a SCALP-05 device, while fracture strength was determined through coaxial double ring testing and evaluated using Weibull statistics. Finite element modeling was used to verify the stress distribution during testing, and Linear Elastic Fracture Mechanics was considered for predicting strength from measured flaw dimensions.
Microscopy and image analysis did not provide conclusive evidence of visible flaw healing after thermal treatment. Most scratches and defects remained detectable, while treatment at 600°C produced bubble-like features on some specimens. The mechanical results showed that the effect of thermal treatment depended on both temperature and the loaded glass surface. For the air side, thermal treatment did not consistently improve the lower-tail strength. For the tin side, treatment at 540°C produced the greatest improvement at low failure probabilities, increasing the failure strength by 33.2% at a failure probability of 0.8% and by 23.1% at 5%. Although treatment at 600°C resulted in a greater increase in median strength, it slightly reduced the strength at the lowest failure probability and introduced additional surface defects.
The laser line scanner was unsuitable for reliable characterization of strength-governing flaws because of transparency, reflectivity, scanning-spray effects, and insufficient spatial and vertical resolution. Consequently, fracture strength could not be reliably predicted from the measured flaw dimensions.
Overall, thermal treatment at approximately 540°C showed the most promising balance between improving the structural reliability of naturally weathered glass and avoiding additional material damage. However, the strength improvement could not be directly related to visible flaw healing, and the investigated non-destructive methods were insufficient for predicting the strength of individual panes.
Investigating Thermal Healing for Glass Reuse
To what extent can thermal treatment enhance the strength of naturally aged glass, affecting their potential for reuse?
Naturally aged glass, developing surface flaws over time from environmental exposure and human activity, was studied alongside artificially aged glass to assess differences in surface damage and thermal treatment effects. Microscopy and image analysis showed that naturally aged glass treated at 500°C and 600°C exhibited no clear healing trend. In contrast, artificially aged glass treated at 500°C caused minimal changes, while at 600°C, scratch width increased due to subcritical crack growth and a yellow discolouration occurred. Energy-dispersive X-ray spectroscopy revealed chemical changes on the air side of the glass, as the metal coating oxidizes during thermal treatment, altering the surface composition.
The strength of aged glass was evaluated using a coaxial double-ring test at 20 MPa/s, with results analysed via the 2-parameter Weibull distribution and weighted least squares regression. The tests revealed clear differences between naturally and artificially aged glass. Thermal treatment reduced the strength of naturally aged glass, with the 5% fractile decreasing by 28% after heating to 500°C and by 56% after heating to 600°C. In contrast, artificially aged glass improved, with the 5% fractile increasing by 13% after heating to 500°C and by 41% after heating to 600°C. SCALP-05 measurements assess surface stress in three groups: untreated glass, and glass treated at 500°C and 600°C. The average surface stresses measured were -6.49 MPa, -2.76 MPa, and -2.30 MPa. Although thermal treatment reduced surface stress, this effect was insufficient to influence overall strength conclusions.
The influence of thermal treatment on surface flaws differs between naturally and artificially aged glass. Microscopy showed minimal changes in naturally aged glass despite reduced strength, while artificially aged glass appeared visually worse but showed strength improvements in strength testing. This is likely due to the primary failure mode: artificially aged glass is strengthened by healing of dominant scratches, whereas naturally aged glass is mainly affected by overall material weakening.
This research assessed whether thermal treatment could restore the strength of naturally aged glass for reuse. However, the results demonstrated that thermal treatment not only failed to enhance the strength of naturally aged glass but also caused a noticeable reduction in strength. Additionally, yellow discolouration occurred during thermal treatment. In conclusion, thermal treatment compromised both the strength and appearance of naturally aged glass, limiting its feasibility for reuse in construction.
...
Naturally aged glass, developing surface flaws over time from environmental exposure and human activity, was studied alongside artificially aged glass to assess differences in surface damage and thermal treatment effects. Microscopy and image analysis showed that naturally aged glass treated at 500°C and 600°C exhibited no clear healing trend. In contrast, artificially aged glass treated at 500°C caused minimal changes, while at 600°C, scratch width increased due to subcritical crack growth and a yellow discolouration occurred. Energy-dispersive X-ray spectroscopy revealed chemical changes on the air side of the glass, as the metal coating oxidizes during thermal treatment, altering the surface composition.
The strength of aged glass was evaluated using a coaxial double-ring test at 20 MPa/s, with results analysed via the 2-parameter Weibull distribution and weighted least squares regression. The tests revealed clear differences between naturally and artificially aged glass. Thermal treatment reduced the strength of naturally aged glass, with the 5% fractile decreasing by 28% after heating to 500°C and by 56% after heating to 600°C. In contrast, artificially aged glass improved, with the 5% fractile increasing by 13% after heating to 500°C and by 41% after heating to 600°C. SCALP-05 measurements assess surface stress in three groups: untreated glass, and glass treated at 500°C and 600°C. The average surface stresses measured were -6.49 MPa, -2.76 MPa, and -2.30 MPa. Although thermal treatment reduced surface stress, this effect was insufficient to influence overall strength conclusions.
The influence of thermal treatment on surface flaws differs between naturally and artificially aged glass. Microscopy showed minimal changes in naturally aged glass despite reduced strength, while artificially aged glass appeared visually worse but showed strength improvements in strength testing. This is likely due to the primary failure mode: artificially aged glass is strengthened by healing of dominant scratches, whereas naturally aged glass is mainly affected by overall material weakening.
This research assessed whether thermal treatment could restore the strength of naturally aged glass for reuse. However, the results demonstrated that thermal treatment not only failed to enhance the strength of naturally aged glass but also caused a noticeable reduction in strength. Additionally, yellow discolouration occurred during thermal treatment. In conclusion, thermal treatment compromised both the strength and appearance of naturally aged glass, limiting its feasibility for reuse in construction.
Niet Nieuw West
A radically circular transformation strategy for a post-war porch flat ensemble
It proposes an alternative method of solving the need for renewal in most post-war housing complexes through a radically circular transformation strategy. This strategy is based on three steps: preserve, reuse, reclaim. A porch flat ensemble in the area of Geuzenveld, Amsterdam Nieuw-West, is used as the design case.
A research was conducted in preparation of the design. It’s main research question: “how can renovation with reclaimed materials become a feasible alternative to reconstruction of the current housing stock?”. From this research, the application of reclaimed insulation and finishing material, was indicated to be highly effective strategies of mitigating the ecological impact of a renovation task. These findings have been incorporated into the design.
The project resulted in a transformation design of the porch flat ensemble that saves 1.808.751 kg CO2-eq and 26.122.919 MJ of energy in terms of material use, relative to a conventional reconstruction design.
...
It proposes an alternative method of solving the need for renewal in most post-war housing complexes through a radically circular transformation strategy. This strategy is based on three steps: preserve, reuse, reclaim. A porch flat ensemble in the area of Geuzenveld, Amsterdam Nieuw-West, is used as the design case.
A research was conducted in preparation of the design. It’s main research question: “how can renovation with reclaimed materials become a feasible alternative to reconstruction of the current housing stock?”. From this research, the application of reclaimed insulation and finishing material, was indicated to be highly effective strategies of mitigating the ecological impact of a renovation task. These findings have been incorporated into the design.
The project resulted in a transformation design of the porch flat ensemble that saves 1.808.751 kg CO2-eq and 26.122.919 MJ of energy in terms of material use, relative to a conventional reconstruction design.
Beyond monotony
Transforming post-war porch flats in Amsterdam Nieuw-West
The design case is located at the Johan Jongkindstraat, close to Lelylaan station.The plot has 6 porch flats with a residential function and 5 smaller buildings with both a residential and public function. The design project forms the location in order to implement the design guidelines provided by the research and forms an example of how to transform in Amsterdam Nieuw-West. The design carefully looked at the design guidelines and implemented them. It also looked at site-specific interventions that were needed to increase living comfort. With the right design interventions, connections were made, repetition was broken, heritage was preserved with new improvements related to current wishes and the entire plan was future-proofed. This project goes beyond monotony and shows that with these interventions, the satisfactory scores in the Western Garden Cities can improve.
...
The design case is located at the Johan Jongkindstraat, close to Lelylaan station.The plot has 6 porch flats with a residential function and 5 smaller buildings with both a residential and public function. The design project forms the location in order to implement the design guidelines provided by the research and forms an example of how to transform in Amsterdam Nieuw-West. The design carefully looked at the design guidelines and implemented them. It also looked at site-specific interventions that were needed to increase living comfort. With the right design interventions, connections were made, repetition was broken, heritage was preserved with new improvements related to current wishes and the entire plan was future-proofed. This project goes beyond monotony and shows that with these interventions, the satisfactory scores in the Western Garden Cities can improve.
Shape optimisation of a second skin
What can be achieved - in terms of structural and building physics performance - when an existing skin of a building is removed and replaced by a new facade
The main driving forces of this thesis are parametric design and optimisation. A parametric design is crucial for this thesis to perform a variation study. Different shapes of the facade are simulated with a custom made genetic algorithm to optimise the shape of the facade. First of all, the cost can be influenced by minimising the amount of material by altering: cross-sections, beam distances, etc. Secondly, by changing the shape of the facade a more aerodynamic building can be created. When the curvature increases, the wind load can be reduced which can make the structure more efficient. The wind load on the facade is determined with the computational fluid dynamics (CFD). The part about building physics focusses on ventilation. A ventilation system is designed which emphasises the importance of integrating the ventilation system with the second skin. The design builds upon the results of the CFD simulation and the structural model. The performance of the system is quantified by determining the usage of natural resources. ...
The main driving forces of this thesis are parametric design and optimisation. A parametric design is crucial for this thesis to perform a variation study. Different shapes of the facade are simulated with a custom made genetic algorithm to optimise the shape of the facade. First of all, the cost can be influenced by minimising the amount of material by altering: cross-sections, beam distances, etc. Secondly, by changing the shape of the facade a more aerodynamic building can be created. When the curvature increases, the wind load can be reduced which can make the structure more efficient. The wind load on the facade is determined with the computational fluid dynamics (CFD). The part about building physics focusses on ventilation. A ventilation system is designed which emphasises the importance of integrating the ventilation system with the second skin. The design builds upon the results of the CFD simulation and the structural model. The performance of the system is quantified by determining the usage of natural resources.
Connecting Glass to Glass with Glass
A Master Thesis on Heat Bonded Glass Connections
The thermal properties of glass can be used to create heat bonds. Heat bonds can be produced in two ways: welding and fusing. With welding, the regions that are to be connected are locally heated. With kiln formed fusing, the elements to be bonded will be globally heated in an oven. This results in the research question: What is the best method, among glass welding and kiln formed glass fusing, to produce heat bonded systems for applications in glass structures?
In theory, safety measures consist of three basic strategies: creating secondary load transfer mechanisms, protectioning and overdimensioning.
These strategies can be used on the scale of the system and the structure. The heat bonded system could theoretically be laminated, reinforced and tempered. On a structural level, safety can be ensured by a combination of the strategies.
To produce glass welds, the glass is preheated in an oven. A small opening in the oven is made and a line burner is used to heat the to be welded area from both sides. One element is pressed down on the other to make the connection. The oven is closed and the specimen is annealed.
Finite element models have been used to analyze thermal shock failure during the weld production process. The recommendations for production were to use an additional flame on the bottom of the specimen or to maintain the surroundings at elevated temperature. The latter option is applied in the experiments.
The results were three transparent, all-glass, soda lime T-shaped objects. Little residual stress remained in the products.
The fused objects were globally heated in an oven. The glass was fused in moulds, made of a gypsum plaster. The products were translucent, all-glass, soda lime, T-shaped objects. The objects deformed significantly during production. Little residual stress remained in the products.
Throughout the experiments, factors have changed. An aspect with no direct influence on the product was quenching after maximum temperature. Adapting the mould and polishing the glass edges prior to fusing had an influence on the objects' shape or texture. None of the factors influenced the order of magnitude of the deformation or the seam between the elements.
A structural test has been performed to compare the specimens with a glass T-shape bonded with transparent UV-curing adhesive. The connections were loaded in shear. The results of the failure loads and stress at failure are of the same order of magnitude. The largest spread was among the fused specimens, the smallest among the welded.
The cause of failure is most probably a combination of elevated stress due to the stiffness and support of the test set-up and peak stress due to irregularities on the glass surface. Other causes could have contributed to failure.
The welded glass product requires most time, energy, skill and money. The adhesive product requires least time and energy. The welded and fused objects had neither acceptable dimensional accuracy, nor a smooth fillet in the joint.
In the current state of development, glass fusion results in less residual stress, requires less skill and is cheaper to produce. Glass welding results in a transparent glass to glass connection and its structural performance is promising. Further research is encouraged into the heat bonded and adhesive connections to create fully transparent connections for structural glass. ...
The thermal properties of glass can be used to create heat bonds. Heat bonds can be produced in two ways: welding and fusing. With welding, the regions that are to be connected are locally heated. With kiln formed fusing, the elements to be bonded will be globally heated in an oven. This results in the research question: What is the best method, among glass welding and kiln formed glass fusing, to produce heat bonded systems for applications in glass structures?
In theory, safety measures consist of three basic strategies: creating secondary load transfer mechanisms, protectioning and overdimensioning.
These strategies can be used on the scale of the system and the structure. The heat bonded system could theoretically be laminated, reinforced and tempered. On a structural level, safety can be ensured by a combination of the strategies.
To produce glass welds, the glass is preheated in an oven. A small opening in the oven is made and a line burner is used to heat the to be welded area from both sides. One element is pressed down on the other to make the connection. The oven is closed and the specimen is annealed.
Finite element models have been used to analyze thermal shock failure during the weld production process. The recommendations for production were to use an additional flame on the bottom of the specimen or to maintain the surroundings at elevated temperature. The latter option is applied in the experiments.
The results were three transparent, all-glass, soda lime T-shaped objects. Little residual stress remained in the products.
The fused objects were globally heated in an oven. The glass was fused in moulds, made of a gypsum plaster. The products were translucent, all-glass, soda lime, T-shaped objects. The objects deformed significantly during production. Little residual stress remained in the products.
Throughout the experiments, factors have changed. An aspect with no direct influence on the product was quenching after maximum temperature. Adapting the mould and polishing the glass edges prior to fusing had an influence on the objects' shape or texture. None of the factors influenced the order of magnitude of the deformation or the seam between the elements.
A structural test has been performed to compare the specimens with a glass T-shape bonded with transparent UV-curing adhesive. The connections were loaded in shear. The results of the failure loads and stress at failure are of the same order of magnitude. The largest spread was among the fused specimens, the smallest among the welded.
The cause of failure is most probably a combination of elevated stress due to the stiffness and support of the test set-up and peak stress due to irregularities on the glass surface. Other causes could have contributed to failure.
The welded glass product requires most time, energy, skill and money. The adhesive product requires least time and energy. The welded and fused objects had neither acceptable dimensional accuracy, nor a smooth fillet in the joint.
In the current state of development, glass fusion results in less residual stress, requires less skill and is cheaper to produce. Glass welding results in a transparent glass to glass connection and its structural performance is promising. Further research is encouraged into the heat bonded and adhesive connections to create fully transparent connections for structural glass.
Where regular float glass is a rather thick, hard and brittle substance that can break easily when subjected to large stresses, thin glass can be found on the other side of the spectrum with its flexibility, clarity and higher strength. Thin glass has rarely been used for architectural applications, mainly because technologies for manufacturing thin glass in construction element sizes were not available or were often too expensive. This product however shows large potential provided sufficient interest is shown from different sectors to lower the price and stimulate innovation. This research will therefore focus on how to implement thin glass on a larger architectural scale and embrace its features to create thinner and stronger load-bearing glazing elements in areas where regular float glass doesn’t work. Several design configuration are proposed, of which the thin glass as cold bent laminated panels is the chosen principle to further explore. The main goal of this research is then to gain insight in the structural and post-breakage behaviour of cold bent laminated thin glass panels. Two layers of Leoflex glass from AGC are to be cold bent into a sinusoidal shape with Saflex DG41 provided by Qdel and SentryGlas provided by Trosifol as the interlayers. From the moment the panels are released from their mould, a certain spring back can be observed. Afterwards, the relaxation phase is initiated. Additionally, experiments are performed on a smaller scale panel for a point load applied in the middle of the upper bent surface. ...
Where regular float glass is a rather thick, hard and brittle substance that can break easily when subjected to large stresses, thin glass can be found on the other side of the spectrum with its flexibility, clarity and higher strength. Thin glass has rarely been used for architectural applications, mainly because technologies for manufacturing thin glass in construction element sizes were not available or were often too expensive. This product however shows large potential provided sufficient interest is shown from different sectors to lower the price and stimulate innovation. This research will therefore focus on how to implement thin glass on a larger architectural scale and embrace its features to create thinner and stronger load-bearing glazing elements in areas where regular float glass doesn’t work. Several design configuration are proposed, of which the thin glass as cold bent laminated panels is the chosen principle to further explore. The main goal of this research is then to gain insight in the structural and post-breakage behaviour of cold bent laminated thin glass panels. Two layers of Leoflex glass from AGC are to be cold bent into a sinusoidal shape with Saflex DG41 provided by Qdel and SentryGlas provided by Trosifol as the interlayers. From the moment the panels are released from their mould, a certain spring back can be observed. Afterwards, the relaxation phase is initiated. Additionally, experiments are performed on a smaller scale panel for a point load applied in the middle of the upper bent surface.
Structural consolidation of historic monuments by interlocking cast glass components
A computational analysis of interlocking cast glass brickwork
The design criteria obtained then are combined into an initial geometry, whose parameters are varied to test their sensitivity to its shear capacity, using FEA. Christensen’s failure criterion is used to locate prone areas in the geometry, and to evaluate the theoretical moment of failure. This output value combines the three principal stresses into a failure envelope, hence can generate contour plots to envision peak-stress-prone areas. This is important especially for glass structures, as they are prone to peak tensile stresses.
From the results design diagrams are created and applied on a conceptual cast glass interlocking consolidation design for the monument chosen as case study: The Lichtenberg Castle ruin.
The initial design is moreover prototyped to check its interlocking capabilities, residual stresses and deviations introduced by shrinkage.
Being able to evaluate possible geometries using FEA can decrease costs and time when searching for a new interlocking geometry. Prone areas are easily highlighted using the Christensen’s failure criterion output. Hence peak stress sensitive or invalid geometries can be discarded before reaching the prototyping stage, which is time consuming and costly.
The creation of a methodology to predict this behaviour is hence valuable for further research on other cast glass geometries and can moreover be applied in any other field when analysing solid complex geometries.
Another goal is to find a cast glass brick design which not only can consolidate the monument of the case study, but is moreover applicable in other projects or configurations. The brick then is not a one-solution design, but can be reused in other projects.
The geometry hence is varied using Grasshopper plug-in for Rhinoceros. By exporting the geometry using a STEP-file, a solid can be loaded into DIANA FEA, where it can be analysed using their newly implemented output value of the Christensen’s failure criterion.
The geometry of the monument is gained through a 3D laser scan, resulting in a point cloud. The point cloud is adapted using Autodesk Recap, then further processed in Rhinoceros.
The Christensen’s failure criterion output is a proper and fast way to evaluate possible cast glass brick designs. Any compressive stresses on the interlocking brick geometry are beneficial for its shear capacity, as is an increase in interlocking amplitude or brick height. Increasing the amplitude however affects the allowable tolerance negatively, which is also the case for a decrease in brick height. Decreasing the brick height hence results in both negative effects.
The conceptual design for consolidation of the Lichtenberg Castle tower can replace the current interventions with equal or higher capacity, even for all conservative assumptions and simplifications. The design can still be altered less conservative after more experimental results and simulations come available.
The methodology applied can now be further developed and performed on other complex geometry designs. The presented multifunctional cast glass interlocking brick design, and its variations can be further investigated and applied in other projects. ...
The design criteria obtained then are combined into an initial geometry, whose parameters are varied to test their sensitivity to its shear capacity, using FEA. Christensen’s failure criterion is used to locate prone areas in the geometry, and to evaluate the theoretical moment of failure. This output value combines the three principal stresses into a failure envelope, hence can generate contour plots to envision peak-stress-prone areas. This is important especially for glass structures, as they are prone to peak tensile stresses.
From the results design diagrams are created and applied on a conceptual cast glass interlocking consolidation design for the monument chosen as case study: The Lichtenberg Castle ruin.
The initial design is moreover prototyped to check its interlocking capabilities, residual stresses and deviations introduced by shrinkage.
Being able to evaluate possible geometries using FEA can decrease costs and time when searching for a new interlocking geometry. Prone areas are easily highlighted using the Christensen’s failure criterion output. Hence peak stress sensitive or invalid geometries can be discarded before reaching the prototyping stage, which is time consuming and costly.
The creation of a methodology to predict this behaviour is hence valuable for further research on other cast glass geometries and can moreover be applied in any other field when analysing solid complex geometries.
Another goal is to find a cast glass brick design which not only can consolidate the monument of the case study, but is moreover applicable in other projects or configurations. The brick then is not a one-solution design, but can be reused in other projects.
The geometry hence is varied using Grasshopper plug-in for Rhinoceros. By exporting the geometry using a STEP-file, a solid can be loaded into DIANA FEA, where it can be analysed using their newly implemented output value of the Christensen’s failure criterion.
The geometry of the monument is gained through a 3D laser scan, resulting in a point cloud. The point cloud is adapted using Autodesk Recap, then further processed in Rhinoceros.
The Christensen’s failure criterion output is a proper and fast way to evaluate possible cast glass brick designs. Any compressive stresses on the interlocking brick geometry are beneficial for its shear capacity, as is an increase in interlocking amplitude or brick height. Increasing the amplitude however affects the allowable tolerance negatively, which is also the case for a decrease in brick height. Decreasing the brick height hence results in both negative effects.
The conceptual design for consolidation of the Lichtenberg Castle tower can replace the current interventions with equal or higher capacity, even for all conservative assumptions and simplifications. The design can still be altered less conservative after more experimental results and simulations come available.
The methodology applied can now be further developed and performed on other complex geometry designs. The presented multifunctional cast glass interlocking brick design, and its variations can be further investigated and applied in other projects.