O. Çelik

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Heating, compaction and cooling phases

Doctoral thesis (2021) - O. Çelik
Thermoplastic composites (TPCs) are emerging in the aerospace industry owing to their advantages over thermoset counterparts such as infinite shelf life, high fracture toughness, chemical and solvent resistance, and recyclability. Also, they are suitable for fast, automated manufacturing since chemical reactions are not required to obtain the final mechanical properties and shape of the TPC structures. Laser-assisted fiber placement (LAFP) has become a promising manufacturing solution with a potential in reducing the material scrap rates and labor time per component, and increasing the repeatibility. Moreover, thanks to the re-melting capability of TPCs, in-situ consolidated (without a post-consolidation step in an oven, press or autoclave) structures can be produced using the LAFP process, which can reduce the capital and energy costs associated with post-consolidation. For the aerospace industry to widely accept and use LAFP with in-situ consolidation, sufficient part quality with a feasible processing speed must be achieved. One of the primary quality indicators is the consolidation quality, which can be quantified by the remaining voids within the composite laminate after manufacturing. Proper consolidation quality can only be obtained once the underlying mechanisms and the relation with the process parameters are understood. The main goal of this thesis is therefore to improve the understanding on the consolidation process during LAFP with in-situ consolidation... ...
Journal article (2021) - Ozan Çelik, S. M.Amin Hosseini, Ismet Baran, Wouter J.B. Grouve, Remko Akkerman, Daniël M.J. Peeters, Julie J.E. Teuwen, Clemens A. Dransfeld
The effect of thermal contact resistance (TCR) correlated to the degree of intimate contact (DIC) between the incoming tape and the substrate on the temperature history during laser-assisted fiber placement (LAFP) was investigated. A novel experimental methodology was designed to understand the effect with a non-contact method which did not influence the local consolidation quality. To assess the influence of TCR numerically, a three-dimensional optical-thermal model was developed. Experimental results indicated that, for the same tape temperature near the nip point, an increase in the compaction force resulted in a decrease in the temperature at the roller exit and the following cooling phase, in correlation with an increase in the final DIC. Also, the effect of the laser power on the final DIC was less pronounced than the compaction force. In the thermal model, when TCR at the tape-substrate interface was not considered, the temperature predictions underestimated the experimental measurements. ...
In this study, the effect of rapid laser heating, which is typical during laser-assisted fiber placement (LAFP), on the micro- and meso- structure of the thermoplastic tape was investigated. Thermoplastic tapes were heated above the melting temperature with different heated lengths (30 and 80 mm and heating times (0.2 and 0.8 s) in a dedicated experimental setup. In-situ and ex-situ characterization techniques were used to observe the differences between the micro- and meso- structure of the tape before and after heating. The experiments resulted in significant changes in the tape structure, namely increased out-of-plane deformation, waviness, arc-length width, roughness, thickness and volumetric void content. This study shows for the first time that a unique deconsolidation behavior takes place during the heating phase of LAFP: the deconsolidation mechanisms are exacerbated by the non-uniform temperature at the tape surface, which is caused by roughness increase and waviness formation. ...
The effects of laser-induced deconsolidation on the compaction process of CF/PEEK tapes were investigated. First, tapes with different degrees of deconsolidation were manufactured using a laser heater. This procedure resulted in samples with different waviness, thickness, void content and surface roughness values. Then, as-received and laser-deconsolidated tapes were compacted under two different temperature histories and four different pressure levels. Waviness induced by laser-deconsolidation vanished when the material was heated up to the glass transition temperature even at a very low compaction pressure. Unlike waviness; increased thickness, void content and surface roughness due to laser-deconsolidation remained between the glass transition and melting temperatures. After the melting temperature was exceeded, the effects of laser-deconsolidation were dependent on the applied pressure and initial degree of deconsolidation. The final surface roughness, thickness and degree of effective intimate contact were affected by the degree of laser-deconsolidation when a compaction pressure of less than 300 kPa was applied. ...

Microstructure and effect of process parameters

Intimate contact development under LAFP-specific thermal and mechanical boundary conditions/interactions and the effect of process parameters are investigated. One-layer, unidirectional strips of CF/PEKK material were placed with different process parameters on a flat tool surface to create different intimate contact conditions. The concept of effective intimate contact, which is based on the resin content at the surface, is introduced and a methodology to measure it from surface micrographs is provided. Degree of effective intimate contact measured from the samples was compared with the existing intimate contact models. The temperature history in the compaction zone was estimated with a finite element model and pressure sensitive films were used to determine the compaction pressure. It is shown that in addition to the squeeze flow mechanism, which is the base for the current intimate contact models, through-thickness percolation flow of the resin needs to be considered to explain the effective intimate contact development. ...
Conference paper (2020) - O. Celik, S.M. Amin Hosseini2, İsmet Baran, Wouter J B Grouve, Remko Akkerman, D.M.J. Peeters, Julie J.E. Teuwen, C.A. Dransfeld
The temperature history during the laser assisted fiber placement (LAFP) process is very important since it significantly influences the final quality of the structure. Air pockets between subsequent plies, caused by the lack of intimate contact, act as insulators and reduce the through-thickness heat transfer. This phenomenon is commonly referred to as the inter-ply thermal contact resistance (TCR). So far, the link between the degree of intimate contact, the corresponding TCR and its influence on the thermal history has not been clearly demonstrated specifically for LAFP. The results indicate that TCR influences the cooling period of the process. ...
Conference paper (2019) - Ozan Celik, Julie J.E. Teuwen
Intimate contact development has been considered as one of the principal mechanisms for consolidation during the automated fiber placement process. This work aims to investigate the effect of process parameters of LAFP on intimate contact development. Effects of nip point temperature, tool temperature, compaction pressure and placement speed on intimate contact development is experimentally investigated. 1-layer, unidirectional strips of CF/PEKK material are placed with different process parameters on a flat tool surface. Based on the observations, the concept of effective intimate contact is introduced and used to assess the degree of intimate contact. The results suggest that the effect of compaction pressure is linear whereas the effects of the placement speed is nonlinear. ...
Laser assisted automated tape or fiber placement (LATP/LAFP) with in-situ consolidation is a promising technique for manufacturing large structures, eliminating the limitations of autoclave curing. Currently, 2-D models are mostly preferred for the thermal analysis of the process. A 3-D, transient thermal finite element model is developed to analyze the effect of the alignment of the heat source with the tape laying direction and is compared with a model imitating a 2-D analysis space. This aspect of the process has not been considered in the literature so far. Effects of this aspect on temperature history and intimate contact evolution are presented. ...