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Freek Bos

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A RILEM TC 304-ADC interlaboratory study — approach and main results

Journal article (2025) - Freek Bos, Costantino Menna, Annika Robens-Radermacher, Rob Wolfs, Nicolas Roussel, Hélène Lombois-Burger, Bilal Baz, Daniel Weger, Yu Chen, More authors...
To show compliance to structural engineering codes and implement quality control measures, it is critical to obtain reliable mechanical properties of the materials in question. For conventional cast and precast concrete, the experimental procedures and relationships between mechanical properties, the material composition, and the production methods are globally known, but for 3D concrete printing (3DCP), these relations have not yet been established. Previous studies have shown little consistency in results, and the underlying experimental methods have not been established broadly. There is an urgent need to address these issues as the application of 3DCP in practice projects is growing rapidly. Therefore, RILEM TC 304-ADC: Assessment of Additively Manufactured Concrete Materials and Structures has set up a large interlaboratory study into the mechanical properties of 3D printed concrete. This paper presents key elements of the experimental approach detailed in the Study Plan and the supporting considerations. Furthermore, it reports on the response, consisting of 34 contributions from 30 laboratories, detailing global coverage, properties of the applied mixture designs and characteristics of the printing facilities that have been used. Subsequently, some fundamental results from compression, flexural, and E-modulus testing are presented and—considering cast specimens as a reference—discussed. On average, a reduction in strength was found in compression and E-modulus (all tested orientations). For flexure, on the other hand, an increase was found in two testing orientations, while a decrease was observed in the third orientation. Importantly, even though the applied experimental methods were found to be reasonably appropriate to obtain the required data, the differences found between individual contributions are significant and sometimes non-consistent, suggesting that testing on specific material-facility combinations is necessary to reliably determine the mechanical properties of objects produced from them. Furthermore, a theoretical framework needs to be developed to further explain the variations that were observed. Extensive analyses of all acquired data are out of the scope of this contribution, but presented in two associated papers, whereas a third presents the data management approach used to process the approximately 5,000 test results. ...
Journal article (2023) - Anne Linde van Overmeir, Branko Šavija, Freek P. Bos, Erik Schlangen
Several studies have shown the potential of strain-hardening cementitious composites (SHCC) as a self-reinforcing printable mortar. However, papers published on the development of three-dimensional printable SHCC (3DP-SHCC) often report a discrepancy between the mechanical properties of the cast and printed specimens. This paper evaluates the effect of each successive phase of the printing process on the mechanical properties of the composite. To this end, materials were collected at three different stages in the printing process, i.e., after each of mixing, pumping, and extruding. The collected 3DP-SHCC materials were then cast in specimen moulds and their mechanical properties after curing were obtained. The resulting findings were juxtaposed with the mechanical properties of the specimens derived from a fully printed 3DP-SHCC element, and our findings indicate that while the density and the compressive strength are not significantly influenced by the printing process, the flexural and tensile strength, along with their associated deflection and strain, are strongly affected. Additionally, this research identifies the pumping phase as the primary phase influencing the mechanical properties during the printing process. ...
Book chapter (2022) - Karsten Nefs, A. L. van Overmeir, Theo A.M. Salet, A. S.J. Suiker, B. Šavija, E. Schlangen, Freek Bos
Previous research has shown that the material properties of a three-dimensional printed strain hardening cementitious composite (3DP-SHCC) can significantly vary, depending on the printing system with which it is produced. However, limited research has been performed on the reproducibility of hardened mechanical properties under identical printing conditions. In this study, the consistency of hardened properties, including compressive strength, flexural strength and deflection, and tensile strength and strain, was tested from materials printed during three separate but identical printing sessions. The research shows that with 3DP-SHCC, significant variations in mechanical properties between printing sessions can be expected. ...
Journal article (2022) - Anne Linde van Overmeir, Stefan C. Figueiredo, Branko Šavija, Freek P. Bos, Erik Schlangen
Since the advent of three-dimensional concrete printing (3DCP), several studies have shown the potential of strain hardening cementitious composites (SHCC) as a self-reinforcing printable mortar. However, only a few papers focus on achieving sufficient buildability when developing printable SHCC. This study investigates the role of the particle size distribution (PSD) in relation to the buildability properties of the mixture in the fresh state and strain hardening properties in the hardened state. To this end 6 mixtures were designed based on optimal particle packing with the application of the Modified Andreasen and Andersen Model. The two mix designs showed the highest displacement at maximum stress were selected for further development of their fresh state rheological properties. This was achieved by addition of a viscosity modifying agent (VMA) and a super plasticizer (SP) and through material analysis by means of ram extrusion tests. Further fresh material characterization on the final two 3DP-SHCC mix designs was attained by the deployment of uniaxial unconfined compression tests (UUCT), Vicat tests and Buildability tests. After successful printing of the two SHCC composites, the compressive strength, the 4-point bending strength and the uniaxial tensile strength and strain were determined at an age of 28 days. The research shows that optimization of the PSD in a 3DP-SHCC mix design results in an improvement of the buildability, but can introduce decreased pumpability and strain hardening capacity. ...
Journal article (2020) - Stefan Chaves Figueiredo, Claudia Romero Rodríguez, Zeeshan Y. Ahmed, Derk H. Bos, Yading Xu, Theo M. Salet, Oguzhan Çopuroglu, Erik Schlangen, Freek P. Bos
Extrusion based additive manufacturing of cementitious materials has demonstrated strong potential to become widely used in the construction industry. However, the use of this technique in practice is conditioned by a feasible solution to implement reinforcement in such automated process. One of the most successful ductile materials in civil engineering, strain hardening cementitious composites (SHCC) have a high potential to be employed for three-dimensional printing. The match between the tailored brittle matrix and ductility of the fibres enables these composites to develop multiple cracks when loaded under tension. Using previously developed mixtures, this study investigates the physical and mechanical performance of printed SHCC. The anisotropic behavior of the materials is explored by means of mechanical tests in several directions and micro computed tomography tests. The results demonstrated a composite showing strain hardening behavior in two directions explained by the fibre orientation found in the printed elements. Moreover, the printing technique used also has guaranteed an enhanced bond in between the printed layers. ...
Conference paper (2020) - Stefan C. Figueiredo, Anne L. van Overmeir, Karsten Nefs, Erik Schlangen, Theo A. M. Salet, Branko Šavija, Akke S. J. Suiker, Freek P. Bos
Over the past few years, several studies have shown the potential of three-dimensional concrete printing (3DCP) for applications in building and civil engineering. However, only a few studies have compared the properties of the fresh printing material and the quality of the printed elements from different printing facilities. Variations in the manufacturing conditions caused by the mixing procedures, the pumping device and the nozzle shape and/or dimensions may influence the quality of the printed elements. This study investigates the differences in the fresh and hardened properties of a printing material tested in two different printing facilities. The pump pressure and temperature experienced by the printing material during the printing session are monitored real-time. Hardened properties are measured for the printed elements, such as the bending capacity, the apparent density, and the air void content. The research shows that two different printing facilities may result in printed elements with relative differences in flexural strength and volumetric density of 49% and 7%, respectively. ...
Journal article (2019) - Stefan Chaves Figueiredo, Claudia Romero Rodríguez, Zeeshan Y. Ahmed, D. H. Bos, Yading Xu, Theo M. Salet, Oğuzhan Çopuroğlu, Erik Schlangen, Freek P. Bos
New additive manufacturing methods for cementitious materials hold a high potential to increase automation in the construction industry. However, these methods require new materials to be developed that meet performance requirements related to specific characteristics of the manufacturing process. The appropriate characterization methods of these materials are still a matter of debate. This study proposes a rheology investigation to systematically develop a printable strain hardening cementitious composite mix design. Two known mixtures were employed and the influence of several parameters, such as the water-to-solid ratio, fibre volume percentage and employment of chemical admixtures, were investigated using a ram extruder and Benbow-Bridgwater equation. Through printing trials, rheology parameters as the initial bulk and shear yield stress were correlated with variables commonly employed to assess printing quality of cementitious materials. The rheology properties measured were used to predict the number of layers a developed mixture could support. Selected mixtures had their mechanical performance assessed through four-point bending, uni-axial tensile and compressive strength tests, to confirm that strain hardening behaviour was obtained. It was concluded that the presented experimental and theoretical framework are promising tools, as the bulk yield stress seems to predict buildability, while shear yield stress may indicate a threshold for pumpability. ...

The design and fabrication of a concrete shell structure

Journal article (2018) - C. Borg Costanzi, Z. Y. Ahmed, H. R. Schipper, F. P. Bos, U. Knaack, R. J.M. Wolfs
One of the geometrical restrictions associated with printed paste materials such as concrete, is that material must be self-supporting during printing. In this research paper a new methodology for 3D Printing Concrete onto a temporary freeform surface is presented. This is achieved by setting up a workflow for combining a Flexible Mould developed at TU Delft with a 4-degrees-of-freedom gantry printer (4 DOF) provided at TU Eindhoven. A number of hypothetical cases are studied, namely fully-printing geometries or combining 3D printing with casting concrete. The final outcome is a 5 m2 partially-printed and partially-cast shell structure, combined with a CNC-milled mould simulating a Flexible Mould. ...