Solder joint reliability related to failures due to thermomechanical loading is a critically important yet physically complex engineering problem. As a result, simulated behavior is oftentimes computationally expensive. In an increasingly data-driven world, it is popular to use efficient data-driven design schemes. Among the family of efficient optimization methods, Bayesian optimization with Gaussian process regression is a key representative. The authors argue that additional computational savings can be obtained from exploiting thorough surrogate modeling and selecting a design candidate based on multiple acquisition functions. This is feasible due to the relatively low computational cost, compared to the expensive simulation objective. This paper presents a novel heuristic framework for performing Bayesian optimization with adaptive hyperparameters across multiple optimization iterations. A comparative study shows the ability of adaptive Bayesian optimization to save on expensive objective evaluations with respect to the worst-performing regular Bayesian optimization scheme. As an engineering use case, the solder joint reliability problem is tackled by minimizing the accumulated non-linear creep strain under a cyclic thermal load. Results show that adaptive Bayesian optimization can at least match the performance of regular Bayesian optimization in terms of raw objective performance, but achieves this with half of the computational expense budget. This practical result underlines the methodological potential of the novel adaptive Bayesian data-driven methodology to achieve more efficient results and significantly cut optimization-related expenses. Lastly, to promote the reproducibility of the results, the data-driven implementations are made available on an open-source basis.

Ultrasensitive and specific detection of low-abundance tumor biomarkers remains a major challenge for early and minimally invasive cancer diagnosis. Here, we present a high-performance biosensing platform that integrates a genetically engineered bacterial S-layer with an AlGaN/GaN high-electron-mobility transistor (HEMT) sensor for label-free detection of tumor antigens. As a proof-of-concept, the ovarian cancer antigen human epididymis protein 4 (HE4) was selected . Specifically, the S-layer protein rSbpA was fused with HE4-specific nanobody 1G8 to construct a bifunctional membrane capable of self-assembling into an ordered biorecognition layer on the sensor surface. Compared to conventional chemical crosslinking, S-layer-driven assembly increased antibody loading by 50 % and minimized nonspecific adsorption in plasma environments. The resulting HEMT sensor detected HE4 across a dynamic linear range (10⁻²¹ to 10⁻¹⁴ M), identifying patients with ovarian cancer with 100 % diagnostic accuracy (AUC = 1.0). This study establishes a versatile and modular biosensing strategy for ultra-low-abundance biomarker detection with broad potential applications in the precision diagnostics of cancer and other diseases.

Residual stress and thermally induced warpage are critical reliability concerns in power electronic packaging, particularly when employing sintered copper nanoparticle (Cu NP) interconnects. While these interconnects provide high thermal and electrical performance, they also introduce significant interfacial stresses during bonding that alter mechanical behavior during service. This study develops an integrated confocal Raman–analytical modeling framework to directly quantify and mechanistically interpret these stresses in a representative SiC/Sintered Cu NPs/Active Metal Brazing ceramic substrate (AMB) stack. Raman spectroscopy reveals a compressive interfacial stress field peaking at −334 MPa near the chip center with localized hotspots linked to microporosity. Complementary in-situ Moiré interferometry tracked warpage evolution during thermal cycle (30–310°C). Coupling this stress measurement with a three-dimensional thermoelastic model, and explicitly assigning the bonding temperature as the stress-free reference, enables accurate reproduction of the temperature-dependent warpage trajectory. The model predictions align with experimental interferometry within < 5% deviation. These results demonstrate that incorporating residual stress is essential to realistically capture thermo-mechanical evolution. The proposed Raman–model paradigm advances beyond prior purely numerical or purely experimental efforts by bridging quantitative stress mapping with predictive warpage modeling. This methodology provides essential insights for thermal-induced residual stress and warpage managements in high-temperature power electronics packaging, providing a stress-informed foundation for reliability assessment and design optimization.

Although silver sintering is widely used in die attach, its reliability under low-pressure and pressureless sintering conditions remains a challenge, and the degradation mechanism needs to be addressed urgently. This study investigates the degradation mechanisms of silver sintered die attach subjected to thermal shock (TS) (−45 °C to 125 °C), revealing its microstructural evolution, degradation of mechanical properties, and pore dynamics. After 1500 cycles, the average porosity did not decrease and remained at approximately 10%, but the porosity distribution exhibited significant heterogeneity, forming three characteristic regions of high porosity, low porosity, and crack regions. With the porosity evolution, the grain size increased by a factor of 2.1–2.8, with the largest grain sizes in the crack region, and the recrystallization fraction decreased significantly, from 89.6 % to a range of 37.3 %–72.1 %. Additionally, the combination with the decrease in both statistically stored dislocation density and total dislocation density reveals a decline in hardness and yield strength of silver sintered layer from 1.05 GPa and 326 MPa to 0.92 GPa and 231 MPa, respectively, gradually diminishing their ability to impede pore migration and merging. Thermal-mechanical coupling simulations based on the actual porous structure images show that the mismatch in the coefficient of thermal expansion induces alternating tensile and compressive thermal stresses, driving pore evolution and crack propagation. The kinetic Monte Carlo (KMC) Potts model based on Kawasaki dynamics combined with pore conservation can effectively predict the long-term pore evolution in this case. These findings provide important guidance for optimizing the sintering process and improving the application of silver sintering materials in high-reliability electronic packaging.

Due to the better performance of the Wide Band Gap (WBG) devices, there has been a paradigm shift toward WBG-based power modules for diverse applications like Electric Vehicles (EVs). However, the high parasitic inductance value of power modules hinders these devices from unlocking their full potential. Therefore, this paper comprehensively reviews SiC-based Single Side Cooling (SSC) power modules that benefit from low parasitic inductance. The paper also discusses the need to develop newer power modules using modern packaging methods. The surveyed power modules are categorized into three main groups, namely wire bonding, hybrid, and 3D packaging methods. This classification contains several vital parameters of the studied power modules, such as nominal and Double Pulse Tests (DPT) power ratings, parasitic inductance, size, etc. The main features and characteristics corresponding to the reviewed power modules' packaging methods and techniques are also briefly described. Finally, a thorough discussion about challenges and future trends is highlighted before concluding the paper.

Pressureless sintered silver paste is widely used in SiC power electronic packaging for its superior thermal and electrical properties, enabling efficient heat dissipation and improved device reliability. Current thermal conductivity models frequently assume isotropic thermal behavior to simplify heat transfer calculations, yet these models neglect the inherent anisotropic porosity of sintered silver materials. This omission introduces errors in the characterization of these materials' thermal performance. This research investigates how the spatial anisotropic distribution of pressureless sintered silver's microstructure impacts QFN packaging's overall thermal conduction performance. This investigation is achieved by comparing lateral/vertical porosity differences between two materials and applying multidimensional thermal conductivity modeling. Two types of pressureless sintered silver were employed as die-attach materials to fabricate SiC MOSFET-based QFN packaging. The sintered microstructures' lateral and vertical cross-sections were characterized using scanning electron microscopy (SEM), enabling quantitative extraction of anisotropic porosity distributions. Subsequently, a numerical model was developed using the extracted porosity data to enhance the accuracy of heat transfer predictions in sintered silver layers while considering anisotropic thermal conductivity. Thermal resistance characterization was conducted on two QFN packages, and the accuracy of the proposed modeling methodology was validated by establishing the interrelation between experimental thermal resistance measurements and theoretical thermal conductivity predictions. This study demonstrates a refined approach to evaluating and optimizing sintered silver materials, providing a more accurate and application-driven thermal management strategy for SiC MOSFET power packaging.

Sintered nano-copper (Cu) improves the thermal performance of SiC MOSFET Fan-Out Panel-Level Packaging (FOPLP), a widely adopted method for miniaturizing electronic systems and modules. This study presented, for the first time, the prototyping and characterization of a 1.2 kV SiC MOSFET FOPLP half-bridge power module using sintered nano-Cu die attachment (FOPLPCu), and compared it with a reference module using conductive Ag adhesive interconnects (FOPLP_Ag). Thermal, mechanical, and electrical co-simulations proved that FOPLPCu exhibited superior performances with lower thermal resistance, power loop parasitic inductance, and thermal deformation, achieving values of 0.14 °C/W (with double-sided cooling), 3.15 nH (@100 kHz), and 9.05e-5 m, respectively. In contrast, FOPLP_Ag showed higher values of 0.24 °C/W, 3.27 nH, and 1.04e-4 m. It is worth noting that due to the higher elastic modulus of sintered nano Cu, FOPLPCu experienced increased thermal stress. The internal structure analysis of the packaged devices, conducted using CSAM, showed that both FOPLPCu and FOPLP_Ag had well-formed interconnections, with no signs of delamination in the EMC, RDL, or interconnect layers. Thermal testing showed that FOPLPCu achieved a single-side thermal resistance of 1.95 °C/W, representing a 22% improvement compared to FOPLP_Ag's 2.5 °C/W. Electrical testing further demonstrated that FOPLPCu had lower on-state resistance compared to FOPLP_Ag, while maintaining comparable breakdown voltage, threshold voltage, and body diode forward voltage drop.

Triboelectric nanogenerator (TENG), advantageous in high energy density and flexibility, is promising as a sustainable energy source but can hardly be used to power edge devices directly due to its high-voltage AC output and varying capacitive impedance. To address it, this work proposes a power-conditioning interface with a fully integrated dual synchronous switch harvesting on capacitors (D-SSHC) rectifier for triboelectric energy extraction. Furthermore, a full digital duty-cycle-based (DCB) maximum power point tracking (MPPT) algorithm is developed to optimize the energy harvesting efficiency with simple implementation and continuous tracking. Designed and fabricated in a 0.18-μm BCD process, the proposed interface can extract energy at a maximum output voltage of 70 V. According to the measurement results, it achieves 99% MPPT efficiency and an energy extraction improvement of 598% compared to a full-bridge rectifier.

While silver-based sintered materials are limited by cost and electromigration, and copper faces challenges with oxidation at high temperatures, Cu-based composite sintering materials offer promising alternative solutions. This review examines recent advances in Cu-based composite sintered materials for die-attach in power electronics packaging, focusing on their mechanical, thermal, electrical properties, and reliability. This review systematically categorizes such compounding strategies, including direct mixing, core-shell structures, and alloying, analyzing the impact on composite properties. Furthermore, the reliability of Cu-based composite sintered joints is evaluated, addressing high-temperature storage, thermal cycling, corrosion, and electrochemical migration. Challenges such as oxidation resistance, process optimization, and cost-effectiveness are discussed, together with future research directions. This work aims to support researchers in advancing Cu-based composite sintering materials research and development, broadening material options for high-temperature power electronics packaging applications.

Silicon-Carbide (SiC) MOSFETs are widely used in high-power and high-efficiency applications such as electric vehicles and power supplies. However, long-term reliability remains a critical concern, particularly under extreme operating conditions. This work aims to explain the health monitoring of SiC metal oxide-semiconductor field effect transistors (MOSFETs) through precise junction temperature (T_j) profiling based on performed measurements. The study focuses on the temperature-dependent behavior of the on-resistance (RDS(on)), a key parameter that varies with the aging, degradation, and temperature of the device. By systematically measuring R_DS(on) at different temperatures and at various stages of the operating life of the device, we can establish a predictive model to assess the health of SiC MOSFETs. The importance of pulse duration of the drain current is stressed to avoid the self-heating effect with some device physics insights. The proposed methodology enables better understanding of the SiC MOSFET performance for future real-time condition monitoring, facilitating early failure detection and lifetime estimation. This approach provides valuable information for improving reliability and optimizing maintenance strategies in power electronics systems. Experimental results validate the effectiveness of the proposed method and give direction for future research opportunities.

The mechanical reliability of sintered silver joints, widely used in power electronics packaging, is critical for long-term applications such as electric vehicle converters. However, conventional homogeneous modeling often oversimplifies internal microstructural variations and limits the accuracy of stress prediction, especially under thermal cycling. In this study, a region-refined modeling framework is proposed to account for epoxy-regulated porosity and mechanical inhomogeneity across the joint. Pressureless die-attach joints were prepared using submicron silver pastes with varying epoxy contents (0∼4 wt%). The joint was divided into five sub-regions from the center to the fillet for localized characterization. Nanoindentation, SEM, and EDS analyses were conducted to assess region-specific mechanical properties and microstructure. Power-law constitutive models were extracted for each region and implemented into finite element simulations of thermal cycling (−55 ∼ 150 °C, 2 cycles/h, 250 h). The sub-region FEM model more accurately captured local stress concentrations and identified failure-prone areas, particularly near the fillet, compared to conventional homogeneous models. Experimental validation confirmed a good correlation between simulated stress zones and observed degradation. This sub-region strategy provides a robust framework for reliability prediction and design optimization of sintered silver joints in high-performance, large-area packaging applications.

This Letter presents a combined analytical and experimental method to effectively decouple the radial and tangential residual stress fields induced by Berkovich nanoindentation in single-crystalline 4H-SiC using micro-Raman spectroscopy. By integrating the Raman stress characterization model with Yoffe’s expanding cavity model, precise extraction of individual residual stress components around the indentation region is realized. Through the vertical backscattering micro-Raman mapping of the E2 phonon mode, we systematically investigate the residual stress distribution near the indentation. The results highlight significant anisotropy in nanoindentation-induced stress fields, strongly dependent on the crystal orientation of 4H-SiC, predominantly featuring radial tensile stress gradients. This comprehensive theoretical–experimental approach offers a robust optical framework for residual stress characterization in 4H-SiC and provides foundational insights for extending Raman spectroscopy-based stress characterization to other crystalline materials and related device structures.

Electronic components are complex systems consisting of a combination of different materials, which undergo degenerative changes over time following the second law of thermodynamics. The loss of their quality or functionality is reflected in degraded performance or behaviour of electronic components, which can lead to failures during their operation lifetime. Thus, it is crucial to understand the physics of material degradation and the factors causing it to ensure component reliability. This paper focuses on the physics-of-degradation of packaging materials, which are typically exposed the most to the environmental and operating loads. The content of this article is organised into three parts. First, an overview of the packaging technology and encapsulating materials is presented. Then, the most common degradation-causing factors and package-associated failure modes are reviewed. Lastly, the hardware requirements are discussed, including specialised sensors, measurement techniques, and Digital Twins, to capture the degradation effects and facilitate component-level health monitoring for microelectronics.

Cold atmospheric plasma (CAP) is widely used in domains such as disinfection, surface treatment and food preservation. When generated in air, CAP is rich in reactive oxygen and nitrogen species (RONS), such as ozone (O3). A dielectric barrier discharge (DBD) is a reliable method to create CAP. We developed a double-sided (twin) surface DBD with novel ‘interfractal’ electrode geometries. This fractal configuration creates stronger electric fields than the customary interdigital line geometry. So, CAP is produced more effectively, resulting in higher RONS concentrations. The performance of interfractal electrodes was compared to that of interdigital electrodes (IDE) in atmospheric air. Nanopulsed powering was used, since it is the most efficient for powering DBDs. Electrical and chemical characteristics (such as ozone level) were assessed. The results show that interfractal electrodes enhance the electric field, conduction current and ozone yield.

The three-step wet etching (TSWE) method has been proven to be a promising technique for fabricating silicon nanopores. Despite its potential, one of the bottlenecks of this method is the precise control of the silicon etching and etch-stop, which results in obtaining a well-defined nanopore size. Herein, we present a novel strategy leveraging electrochemical passivation to achieve accurate control over the silicon etching process. By dynamically controlling the oxide layer growth, rapid and reliable etch-stop was achieved in under 4 s, enabling the controllable fabrication of sub-10 nm silicon nanopores. The thickness of the oxide layer was precisely modulated by adjusting the passivation potential, achieving nanopore size shrinkage with a precision better than 2 nm, which can be further enhanced with more refined potential control. This scalable method significantly enhances the TSWE process, offering an efficient approach for producing small-size silicon nanopores with high precision. Importantly, the precise etching control facilitated by electrochemical passivation holds promise for the cost-effective production of high-density, air-insulated monolithic integrated circuits. (Figure presented.)

This work investigated the impact of die-attach fillet geometry on the reliability of epoxy-based pressure-less sintered silver joints. Three types of sintered silver samples (Ag-0, Ag-1, and Ag-2) with 0%, 1%, and 2% epoxy content were prepared and characterized. Nanoindentation tests combined with inverse calculations were used to determine their elasto-plastic behavior. Fillet formation was influenced by organic solvent composition, dispense volume, and placement pressure, resulting in three geometries: rounded, triangular, and rounded rectangular. Finite element analysis was employed to simulate stress distribution and equivalent thermal strain under thermal cycling conditions (−55°C to 150°C). The simulation results were validated experimentally through shear strength testing and microstructural characterization using scanning electron microscopy (SEM). The findings highlight the significant role of fillet geometry, climbing height, and die-attach thickness in stress distribution and failure mechanisms, providing valuable insights into optimizing the die-attach process to enhance joint reliability in power electronics applications.

This paper investigates the effects of three ageing factors (chemical, humidity, and temperature) and their interactions on the physical properties and degradation of silicone sealant used in microelectronic applications. The thermal degradation of silicone sealants was investigated by exposing samples to temperatures in the range of 150 up to 175 °C. Also, a set of samples were aged at 40 °C in a salt spray set-up with 100 % humidity in a salty atmosphere. Results showed detectable changes in the FTIR spectra of aged specimen as compared with the as-received sample. In all accelerated testing conditions, peak intensities decreased with ageing time, inferring that that the surface characteristics of the sealant is affected by ageing. Shear test results showed that with increasing the ageing time, the maximum shear stress in most cases has decreased in all ageing conditions. Also, it appears that samples with longer ageing times have experienced more elongation before failure. Results also show that salt spraying of specimens is associated with a decrease in the mechanical properties of the sealant, indicating the deleterious implications of ionic contaminations for the mechanical properties of samples.

This study investigates the interface strength and fracture behavior of sintered copper (Cu) nanoparticles (NPs) for all-Cu integration in advanced microelectronics packaging. Micro-cantilever bending tests on three configurations (Cu NP-notched, interface-notched and un-notched micro-cantilevers) were analyzed using scanning electron microscopy (SEM), transmission electron microscopy (TEM), transmission Kikuchi diffraction (TKD) and cohesive zone model (CZM). The interface-notched micro-cantilevers demonstrate superior fracture resistance, with a stress intensity factor (K_Q) of 2.88±0.10 MPa m^1/2, compared to 2.12±0.11 MPa m^1/2 for Cu NP-notched micro-cantilevers. Simulation results, consistent with experimental results, reveal that Cu NP-notched micro-cantilevers exhibit lower fracture resistance due to porosity and stress concentrations, while interface-notched micro-cantilevers show enhanced strength, attributed to robust bonding and reduced void distribution. Un-notched micro-cantilevers display superior load-bearing capacity, with cracks bypassing the interface and propagating through porous regions. Moreover, in un-notched micro-cantilevers, a synergistic deformation mechanism is observed, where crack propagation through the sintered Cu NPs coexists with plastic slip deformation in the Cu substrate. These findings highlight the strong interfacial bonding and effective stress transfer at the Cu substrate-sintered Cu NP interface, validating the feasibility of direct sintering using Cu NPs without additional coatings.

This study presents a novel approach for localized silver (Ag) nanoparticles (NPs) sintering using microheater arrays embedded within the Si substrate. By applying controlled pulse currents, these microheaters generate targeted heat pulses, enabling rapid and localized sintering while maintaining the surrounding device components at room temperature. This localized heating minimizes thermal stress caused by thermal expansion mismatches, as sintering completes within milliseconds. Compared to conventional sintering techniques, this method improves process efficiency, reduces power consumption, and provides precise spatial control over the sintered regions. The proposed approach offers a promising alternative for microelectronics packaging and integration, particularly in applications requiring precise thermal management.

The mechanical strength of sintered nanoparticles (NPs) limits their application in advanced electronics packaging. In this study, we explore the anisotropy in the microstructure and mechanical properties of sintered copper (Cu) NPs by combining experimental techniques with molecular dynamics (MD) simulations. We establish a clear relationship between processing conditions, microstructural evolution, and resulting properties in pressure-assisted sintering of Cu NPs. Our findings reveal that pressure-assisted sintering induces significant anisotropy in the microstructure, as evidenced by variations in areal relative density and the orientation distribution of necks formed during sintering. Specifically, along the direction of applied pressure, the microstructure exhibits reduced variation in areal relative density and a higher prevalence of necks with favorable orientations. The resulting anisotropic mechanical properties, with significantly higher strength along the pressure direction compared to other directions, are demonstrated through micro-cantilever bending tests and tensile simulations. This anisotropy is further explained by the combined effects of strain localization (influenced by areal relative density) and the failure modes of necks (determined by their orientation relative to the loading direction). This work provides valuable insights into the analysis of sintered NPs microstructures and offers guidance for optimizing the sintering process.